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Lim Bee Ying
Preferred name
Lim Bee Ying
Official Name
Lim, Bee Ying
Alternative Name
Lim, B. Y.
Lim, Bee Y.
Main Affiliation
Scopus Author ID
57209532691
Researcher ID
DVB-1384-2022
Now showing
1 - 10 of 19
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PublicationEffect of solvent on mechanical and physical properties of PMMA/Sic composite films( 2024-12)
;Auni Fakhira Che Baharudin ; ; ;The selection of solvent in solution casting is crucial as it may affect the morphology and properties of the resulting composite films. In this study, the effect of solvent on the properties of poly(methyl methacrylate)/silicon carbide (PMMA/SiC) composite films was investigated. By using acetone, the solution casting was carried out at various solvent-to-solid (S/S) ratio, from 4:1 to 10:1 at room temperature. It was found that the increasing S/S ratio enhanced the tensile strength and modulus of elasticity of pristine PMMA films but deteriorated its elongation at break, up to 8:1 ratio. The crystallinity of the PMMA films was found to increase with S/S ratio, as confirmed by the higher peak intensity in X-Ray Diffraction (XRD) patterns and the SEM micrographs. In the second part of the study, by using S/S ratio of 8:1, the nano sized SiC (0.25 wt%) was added as a filler into PMMA and toluene with different ratio was added as a secondary solvent. The addition of SiC has increased the tensile strength and modulus of elasticity of PMMA/SiC but decreased its elongation at break. However, the presence of toluene reduced the tensile strength of the PMMA/SiC composite films and resulting in rougher tensile fracture surfaces as shown in SEM micrographs. The toluene with nonpolar nature had affected the distribution of SiC in PMMA. It can be concluded that the properties of the PMMA composites films can be tailored according to the needs of applications. -
PublicationFabrication of polymethyl methacrylate composite films with silanized SiC nanoparticles( 2025-01)
;Mohamad Azrol Bin Azmi ; ; ;Phey Yee FoongThe properties of polymeric composites have often been altered with the incorporation of fillers. In this study, the poly(methyl methacrylate) (PMMA) was filled with silicon carbide nano-particles (SiC). The PMMA/SiC composite films were prepared through solution casting by using acetone as solvent. The different loading of SiC ranging from 0.25 wt% to 1.00 wt% were incorporated into the PMMA matrix. The effect of SiC loading and silane coupling agent on PMMA/SiC composite films in terms of mechanical, physical, and morphological properties was investigated. It was found that the increasing SiC loading and the silane treatment had increased the tensile strength and Young’s modulus but reduced the elongation at the break of PMMA/SiC composite films. At 0.75 wt% of silanized SiC, the tensile strength of the composite films was found to increase by 25 % from 30 to 37.5 MPa as compared to the virgin PMMA. Besides, the hardness of composite films was also increased with SiC loading and silane treatment. The presence of 1.00 wt% silanized SiC had increased 21.7% the hardness of the virgin PMMA, resulting in the increase of Shore A value from 69 to 84. By using silane treatment, better filler-matrix interaction was established as smoother fracture surfaces were observed through SEM micrographs and higher d-spacing was found in X-ray diffraction (XRD) patterns. The PMMA/SiC composite films prepared were suitable to be used in sporting goods, additive manufacturing, and environmental and protective coatings. -
PublicationThe effect of coated calcium carbonate using stearic acid on the recovered carbon black masterbatch in low-density polyethylene composites( 2023-01-01)
;Leow V.J. ; ;Yeoh C.K. ; ;Wong W.C. ; ;Mohamed Rasidi M.S.This research focuses on recycling rubber tire waste through pyrolysis to produce recovered carbon black (rCB). The rCB is combined with recycled low-density polyethylene (rLDPE), calcium carbonate (CaCO3), fatty acid, metallic stearate, and polyethylene (PE) wax to create an rCB masterbatch for household packaging. Surface modification of CaCO3 particles using stearic acid improves the compatibility with LDPE. The study investigates mechanical properties, morphology, melt flow index (MFI), X-ray diffraction, and thermogravimetric analysis in three systems: uncoated, coated, and a hybrid combination of coated and uncoated CaCO3 in LDPE/rCB masterbatch composites. The coated system demonstrates higher mechanical properties and improved compatibility between CaCO3 and LDPE. All three systems exhibit enhanced thermal stability and MFI compared to virgin LDPE, with the coated system showing the most significant improvement. The study showcases the potential of LDPE/rCB masterbatch composites for household packaging, with the coated system displaying the optimum performance across various characteristics.1 33 -
PublicationEffect of solvent to matrix weight ratio and stearic acid treatment on the mechanical properties of Poly (methyl methacrylate)/ palm kernel shell composites( 2021-07-21)
; ; ;Lye S.F.In this study, poly (methyl methacrylate)/palm kernel shell (PMMA/PKS) composites were prepared by solution casting. The effect of solvent to matrix (S/M) weight ratio and stearic acid (SA) treatment on PMMA/PKS composites were studied. PMMA pellets were dissolved and PKS powders were dispersed into acetone, separately. PMMA solution and PKS suspension were then mixed in ultrasonic bath. The mixture was then poured into a glass petri dish to evaporate acetone at room temperature and finally PMMA/PKS composite thin film was obtained. PMMA/PKS composites were characterized by using SEM and were subjected to tensile test. It was found that tensile strength, modulus of elasticity of composite increased but elongation at break decreased with the increasing S/M ratio and with SA treatment. The improvement of the mechanical properties was due to the improved interfacial bonding following the SA treatment and the formation of crystallized PMMA domain in the composite with the increasing S/M ratio. SEM images revealed even fracture surfaces as S/M increased and with the application of SA treatment that indicate better matrix-filler adhesion. It can be concluded that S/M increment and SA treatment improved mechanical properties of PMMA/PKS composite.20 8 -
PublicationSynthesis and preparation of metal oxide powders( 2020-01-01)
; ; ; ;Al-Douri Y.In recent years, metal oxide, especially in the form of powders, is extensively studied owing to their unique and novel properties. In this regard, this chapter provides a thorough description of current advances on the synthesis and preparation of metal oxide powders. The chapter begins with the introduction and motivation of the preparation of synthetic metal oxide powders. This is followed by the description of the synthesis and preparation method of metal oxide powders, which can be categorized into chemical methods, physical methods, and biological methods. Several important methods under each category were described with examples. This chapter ends with concluding remarks with views on the recent progress and future challenges of metal oxide powders research.4 21 -
PublicationMicrowave welding of thermoplastic using silicon carbide nanowhiskers as susceptor effect of heating duration( 2024-06)
;Phey Yee Foong ; ; ; ; ; ; ; ;Foo Wah Low ;Muhammad Kashif ;Nor Azura Abdul Rahman ;Veeradasan PerumalMicrowave welding is becoming more popular than conventional joining methods due to its advantages such as rapid and localised heating as well as applicable to components with complicated geometry. Previously reported susceptor, such as carbonaceous materials and conductive polymers, are toxic and the welding process involving these susceptors is time-consuming. Because of its exceptional microwave absorption and biocompatibility, silicon carbide nanowhiskers (SiCNWs) was employed as the microwave susceptor for microwave welding. Microwave welding in this study comprises of only three simple steps: SiCNWs suspension preparation, SiCNWs application and microwave heating. The weld strength of welded joint was then characterised using tensile test and energy dispersive x-ray spectroscopy equipped scanning electron microscopy (EDS-SEM) to study its mechanical properties and cross-section microstructure. The influence of microwave irradiation time was studied in this study, and it is found that the weld strength rose with the extension of microwave irradiation time, until a maximum weld strength of 1.61 MPa was achieved by 17 s welded joint. The development of SiCNWs reinforced PP nanocomposite welded joint layer is responsible for the enhanced weld strength. Prolonged heating duration may also result in flaws such as void formation at the welded joint, which subsequently lowered the weld strength to 0.60 MPa when the heating duration was extended to 20 s. In sum, a strengthen welded joint can be formed with rapid microwave heating under the proper control of heating duration.10 49 -
PublicationThe effect of graphite type on the synthesis of SiC nanomaterials by microwave-assisted synthesis( 2020-09-01)
;Mat Kahar Suhaimi ; ; ;Al-Douri Y. ; ;Ten S.T. ; ;SiC nanomaterial (SiCNM) is known for its excellent properties and has great potential for a wide range of applications. In this article, preparation of SiCNMs from different types of graphite was performed by microwave-assisted synthesis. Different types of graphite which are graphite flake (GF) and expanded graphite (EG) were used to react with silica for the synthesis of SiCNMs in laboratory microwave furnace at 1400 °C. It was found that SiC nanowhiskers (SiCNWs) were formed when EG was used, while irregular shaped SiC nanoparticles (SiCNPs) were formed when GF was used. β-SiC appeared as the only phase in the XRD patterns for both SiCNMs formed using GF and EG. SiCNWs and SiCNPs have interplanar spacing of around 0.25 nm which is the axial direction of [111]. The difference of formation mechanism is believed to be the origin of different morphology of SiCNMs synthesized from different types of graphite.3 22 -
PublicationPreparation and characterization of tensile properties of PMMA-SiC nanowhiskers nanocomposite films: effect of filler loading and silane treatment( 2023-10)
; ; ;L. Y. Lee ;P. Y. FoongThe preparation of nanocomposites through melt mixing was challenging as the nanofillers tend to form agglomeration. The silicon carbide nanowhiskers (SiCNWs) filled poly (methyl methacrylate) (PMMA) thin film in this study was prepared by means of solution casting. Acetone with low toxicity was used as solvent to dissolve the PMMA pellets. A coupling agent, silane was used to enhance the properties of composite films. Besides, the untreated and treated SiCNWs were filled into PMMA matrix, respectively with the filler loading varied from 0.2 to 0.8 wt%. The universal testing machine was used to investigate the tensile properties of composites. It was found out that the tensile strength of the PMMA was reduced in the presence of SiCNWs. However, the tensile strength had increased with the rise of filler loading. At 0.8 wt% of SiCNWs, the composites’ tensile strength was comparable to virgin PMMA. Meanwhile, the SiCNWs had reduced the elongation at break but increased the elastic modulus of PMMA/SiCNWs nanocomposite films. In addition, silane surface treatment on SiCNWs had improved the tensile strength and ductility but lowered the elastic modulus of the nanocomposites. The improvement was due to the enhancement of interfacial adhesion between SiCNWs and PMMA.7 13 -
PublicationMicrowave Welding of Thermoplastic using Silicon Carbide Nanowhiskers as Susceptor: Effect of Heating Duration( 2024-06-01)
;Foong P.Y. ; ; ; ; ; ; ;Low F.W. ; ;Kashif M. ;Rahman N.A.A. ;Perumal V.Microwave welding is becoming more popular than conventional joining methods due to its advantages such as rapid and localised heating as well as applicable to components with complicated geometry. Previously reported susceptor, such as carbonaceous materials and conductive polymers, are toxic and the welding process involving these susceptors is time-consuming. Because of its exceptional microwave absorption and biocompatibility, silicon carbide nanowhiskers (SiCNWs) was employed as the microwave susceptor for microwave welding. Microwave welding in this study comprises of only three simple steps: SiCNWs suspension preparation, SiCNWs application and microwave heating. The weld strength of welded joint was then characterised using tensile test and energy dispersive x-ray spectroscopy equipped scanning electron microscopy (EDS-SEM) to study its mechanical properties and cross-section microstructure. The influence of microwave irradiation time was studied in this study, and it is found that the weld strength rose with the extension of microwave irradiation time, until a maximum weld strength of 1.61 MPa was achieved by 17 s welded joint. The development of SiCNWs reinforced PP nanocomposite welded joint layer is responsible for the enhanced weld strength. Prolonged heating duration may also result in flaws such as void formation at the welded joint, which subsequently lowered the weld strength to 0.60 MPa when the heating duration was extended to 20 s. In sum, a strengthen welded joint can be formed with rapid microwave heating under the proper control of heating duration.1 21 -
PublicationEffect of dispersibility of graphene nanoplatelets on the properties of natural rubber latex composites using sodium dodecyl sulfate(Walter de Gruyter GmbH, 2022-01-01)
;Che W.M. ; ; ; ;Rasidi M.S.M.Natural rubber latex/graphene nanoplatelet (NRL/GNP) composites containing GNP-pristine and GNP-SDS were prepared by a simple mechanical mixing method. The main objective was to study the effect of dispersibility of GNP on the properties in NRL. X-ray diffraction confirmed the adsorption of sodium sulfate dodecyl (SDS) on the GNP surface. The results showed that high filler loading diminished the physical and mechanical properties of the composites but successfully endured to satisfy electrical conductivity to the NRL/GNP composites. Besides, the SDS surfactant-filled system demonstrated better physical, tensile, electrical, and thermal stability properties than the GNP-pristine. The intercalated and dispersed GNP-SDS increased the number of routes for stress and heat transfer to occur and facilitated the formation of conductive pathways as well, leading to the improvement of the properties as compared to NRL/GNP-pristine composites. However, as the GNP-SDS loading exceeded 5 phr, the GNP-SDS localized in the interstitial layer of NRL, restricted the formation of crosslinking, and interfered with the strain-induced crystallization ability of the composites.3 2