Mohd. Mustafa Al Bakri Abdullah
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Preferred name
Mohd. Mustafa Al Bakri Abdullah
Official Name
Abdulah, Mohd. Mustafa Al Bakri
Alternative Name
Abdullah, M.M.A.
M.M.A. Abdullah
Mustafa Al Bakri, A. M.
Albakri Abdullah, M. M.
Main Affiliation
CeGeoGTech UniMAP
Scopus Author ID
53164519100

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  • Publication
    Crumb rubber geopolymer mortar at elevated temperature exposure
    ( 2022)
    Ahmad Azrem Azmi
    ;
    Mohd. Mustafa Al Bakri Abdullah
    ;
    Che Mohd Ruzaidi Ghazali
    ;
    Romisuhani Ahmad
    ;
    Ramadhansyah Putra Jaya
    ;
    Shayfull Zamree Abd. Rahim
    ;
    Mohammad A. Almadani
    ;
    Wysłocki, Jerzy J.
    ;
    Agata Åšliwa
    ;
    Andre Victor Sandu
    Low calcium fly ash is used as the main material in the mixture and the crumb rubber was used in replacing fine aggregates in geopolymer mortar. Sodium hydroxide (NaOH) and sodium silicate (Na2SiO3) which were high alkaline solution were incorporated as the alkaline solution. The fly ash reacted with the alkaline solution forming alumino-silicate gel that binds the aggregate to produce a geopolymer mortar. The loading of crumb rubber in the fly ash based geopolymer mortar was set at 0%
  • Publication
    Microstructural studies of Ag/TiO2 thin film; effect of annealing temperature
    ( 2021)
    Kamrosni Abdul Razak
    ;
    C.H. Dewi Suryani
    ;
    A. Azliza
    ;
    Mohd. Mustafa Al Bakri Abdullah
    ;
    Mohd Arif Anuar Mohd Salleh
    ;
    Norsuria Mahmed
    ;
    V. Chobpattana
    ;
    L. Kaczmarek
    ;
    B. Jeż
    ;
    M. Nabiałek
    Microstructures are an important link between materials processing and performance, and microstructure control is essential for any materials processing route where the microstructure plays a major role in determining the properties. In this work, silverdoped titanium dioxide (Ag/TiO2) thin film was prepared by the sol-gel method through the hydrolysis of titanium tetra-isopropoxide and silver nitrate solution. The sol was spin coated on ITO glass substrate to get uniform film followed by annealing process for 2 hours. The obtained films were annealed at different annealing temperatures in the range of 300°C-600°C in order to observe the effect on crystalline state, microstructures and optical properties of Ag/TiO2 thin film. The thin films were characterized by X-Ray diffraction (XRD), scanning electron microscopy (SEM), and UV-Vis spectrophotometry. It is clearly seen, when the annealing temperature increases to 500°C, a peak at 2θ = 25.30° can be seen which refers to the structure of TiO2 tetragonal anatase. The structure of Ag/TiO2 thin film become denser, linked together, porous and uniformly distributed on the surface and displays the highest cut-off wavelength value which is 396 nm with the lowest band gap value, which is 3.10 eV. Keywords: Ag/TiO2; Annealing Temperature; Microstructure; Optical Properties; Thin Film
  • Publication
    Synthesis of metakaolin based alkali activated materials as an adsorbent at different Na2SiO3/NaOH ratios and exposing temperatures for Cu2+ Removal
    ( 2023)
    Masdiyana Ibrahim
    ;
    Wan Mastura Wan Ibrahim
    ;
    Mohd. Mustafa Al Bakri Abdullah
    ;
    Marcin Nabialek
    ;
    Ramadhansyah Putra Jaya
    ;
    Monthian Setkit
    ;
    Romisuhani Ahmad
    ;
    Bartłomiej Jeż
    Water contamination is a major issue due to industrial releases of hazardous heavy metals. Copper ions are among the most dangerous heavy metals owing to their carcinogenicity and harmful effects on the environment and human health. Adsorption of copper ions using alkali activated materials synthesized through the polycondensation reaction of an alkali source and aluminosilicates is the most promising technique, and has a high adsorption capability owing to a large surface area and pore volume. This research focuses on the effect of the alkaline activator ratio, which is a sodium silicate to sodium hydroxide ratio. Various exposing temperatures on metakaolin based alkali activated materials on a surface structure with excellent functional properties can be used as adsorbent materials for the removal of copper ions. A variety of mix designs were created with varying sodium silicate to sodium hydroxide ratios, with a fixed sodium hydroxide molarity, metakaolin to alkali activator ratio, hydrogen peroxide, and surfactant content of 10 M, 0.8, 1.00 wt%, and 3.0 wt%, respectively. Most wastewater adsorbents need high sintering temperatures, requiring an energy-intensive and time-consuming manufacturing process. In this way, metakaolin-based alkali activated materials are adsorbent and may be produced easily by solidifying the sample at 60 °C without using much energy. The specific surface area, water absorption, microstructure, phase analysis, functional group analysis, and adsorption capability of copper ions by metakaolin based alkali activated materials as adsorbents were evaluated. The water absorption test on the samples revealed that the sodium silicate to sodium hydroxide 0.5 ratio had the highest water absorption percentage of 36.24%, superior pore size distribution, and homogeneous porosity at 60 °C, with a surface area of 24.6076 m2/g and the highest copper ion uptake of 63.726 mg/g with 95.59% copper ion removal efficiency at adsorption condition of pH = 5, a dosage of 0.15 g, 100 mg/L of the initial copper solution, the temperature of 25 °C, and contact time of 60 min. It is concluded that self-supported metakaolin based alkali activated material adsorbents synthesized at low temperatures effectively remove copper ions in aqueous solutions, making them an excellent alternative for wastewater treatment applications.
  • Publication
    Properties of stone mastic asphalt incorporating nano titanium as binder's modifier
    ( 2022)
    Nur Syafiqah Shamimi Mohd Zali
    ;
    Khairil Azman Masri
    ;
    Ramadhansyah Putra Jaya
    ;
    Mohd. Mustafa Al Bakri Abdullah
    ;
    Muzamir Hasan
    ;
    Mohd Rosli Mohd Hasan
    ;
    Bartłomiej Jeż
    ;
    Marcin Nabiałek
    ;
    Marek Sroka
    ;
    Paweł Pietrusiewicz
    Stone mastic asphalt is a gap-graded mix and is usually related to its high bitumen content and its skeleton-like constitution. Although famous for its durability, high resistance to fatigue and rutting, issues such as bleeding and premature aging do occur in the mix since it has a high bitumen content and voids due to its gap-graded structure. In order to encounter these problems from affecting the mix, some instances such as adding additives, rejuvenators and stabilizers into the mixture has been implemented. Nowadays, nano materials are being used in the asphalt mixtures and nano titanium is being introduced as a modifier to the asphalt binder in order to improve the mechanical properties of the stone mastic asphalt mix. The related tests done in order to access the improvement are resilient modulus, dynamic creep, moisture susceptibility and binder drain down. The content of nano titanium used in this research are 1%, 2%, 3%, 4% and 5%. This study is done to assess the mechanical performance of stone mastic asphalt with nano titanium modified binder.
  • Publication
    Microstructure evolution of Ag/TiO2 thin film
    ( 2021)
    Dewi Suriyani Che Halin
    ;
    Kamrosni Abdul Razak
    ;
    Mohd Arif Anuar Mohd Salleh
    ;
    Mohd Izrul Izwan Ramli
    ;
    Mohd. Mustafa Al Bakri Abdullah
    ;
    Ayu Wazira Azhari
    ;
    Kazuhiro Nogita
    ;
    Hideyuki Yasuda
    ;
    Marcin Nabiałek
    ;
    Jerzy J. Wysłocki
    Ag/TiO2 thin films were prepared using the sol-gel spin coating method. The microstructural growth behaviors of the prepared Ag/TiO2 thin films were elucidated using real-time synchrotron radiation imaging, its structure was determined using grazing incidence X-ray diffraction (GIXRD), its morphology was imaged using the field emission scanning electron microscopy (FESEM), and its surface topography was examined using the atomic force microscope (AFM) in contact mode. The cubical shape was detected and identified as Ag, while the anatase, TiO2 thin film resembled a porous ring-like structure. It was found that each ring that coalesced and formed channels occurred at a low annealing temperature of 280 °C. The energy dispersive X-ray (EDX) result revealed a small amount of Ag presence in the Ag/TiO2 thin films. From the in-situ synchrotron radiation imaging, it was observed that as the annealing time increased, the growth of Ag/TiO2 also increased in terms of area and the number of junctions. The growth rate of Ag/TiO2 at 600 s was 47.26 µm2/s, and after 1200 s it decreased to 11.50 µm2/s and 11.55 µm2/s at 1800 s. Prolonged annealing will further decrease the growth rate to 5.94 µm2/s, 4.12 µm2/s and 4.86 µm2/s at 2400 s, 3000 s and 3600 s, respectively.
  • Publication
    Influence of 1.5 wt.% Bi on the microstructure, hardness, and shear strength of Sn-0.7Cu solder joints after isothermal annealing
    ( 2021)
    Mohd Izrul Izwan Ramli
    ;
    Mohd Arif Anuar Mohd Salleh
    ;
    Andrei Victor Sandu
    ;
    Siti Farahnabilah Muhd Amli
    ;
    Rita Mohd Said
    ;
    Norainiza Saud
    ;
    Mohd. Mustafa Al Bakri Abdullah
    ;
    Petrica Vizureanu
    ;
    Adam Rylski
    ;
    Jitrin Chaiprapa
    ;
    Marcin Nabialek
    This manuscript reports the isothermal annealing effect on the mechanical and microstructure characteristics of Sn-0.7Cu-1.5Bi solder joints. A detailed microstructure observation was carried out, including measuring the activation energy of the intermetallic compound (IMC) layer of the solder joints. Additionally, the synchrotron µX-ray fluorescence (XRF) method was adopted to precisely explore the elemental distribution in the joints. Results indicated that the Cu6Sn5 and Cu3Sn intermetallic layers thickness at the solder/Cu interface rises with annealing time at a rate of 0.042 µm/h for Sn-0.7Cu and 0.037 µm/h for Sn-0.7Cu-1.5Bi. The IMC growth’s activation energy during annealing is 48.96 kJ mol-1 for Sn-0.7Cu, while adding Bi into Sn-0.7Cu solder increased the activation energy to 55.76 kJ mol−1. The µ-XRF shows a lower Cu concentration level in Sn-0.7Cu-1.5Bi, where the Bi element was well dispersed in the β-Sn area as a result of the solid solution mechanism. The shape of the IMC layer also reconstructs from a scallop shape to a planar shape after the annealing process. The Sn-0.7Cu hardness and shear strength increased significantly with 1.5 wt.% Bi addition in reflowed and after isothermal annealing conditions.
  • Publication
    Effect of NaOH molar concentration on microstructure and compressive strength of Dolomite/Fly Ash-Based geopolymers
    ( 2021)
    Emy Aizat Azimi
    ;
    M.A.A. Mohd Salleh
    ;
    Mohd. Mustafa Al Bakri Abdullah
    ;
    Ikmal Hakem A. Aziz
    ;
    Kamarudin Hussin
    ;
    Jitrin Chaiprapa
    ;
    Petrica Vizureanu
    ;
    Sorachon Yoriya
    ;
    Marcin Nabiałek
    ;
    Jerzy J. Wyslocki
    Dolomite can be used as a source of aluminosilicate to produce geopolymers; however, this approach is limited by its low reactivity. This study analyzes the viability of producing geopolymers using dolomite/fly-ash with sodium silicate and NaOH solutions (at multiple concentrations) by determining the resultant geopolymers’ compressive strengths. The dolomite/fly-ash-based geopolymers at a NaOH concentration of ~22 M resulted in an optimum compressive strength of 46.38 MPa after being cured for 28 days, and the SEM and FTIR analyses confirmed the denser surface of the geopolymer matrix. The synchrotron micro-XRF analyses confirmed that the Ca concentration exceeded that of Si and Mg, leading to the formation of calcium silicate hydrate, which strengthens the resulting geopolymers.
  • Publication
    Assessment of the suitability of ceramic waste in geopolymer composites: an appraisal
    ( 2021)
    Ismail Luhar
    ;
    Salmabanu Luhar
    ;
    Mohd. Mustafa Al Bakri Abdullah
    ;
    Marcin Nabiałek
    ;
    Andrei Victor Sandu
    ;
    Janusz Szmidla
    ;
    Anna Jurczyńska
    ;
    Rafiza Abdul Razak
    ;
    Ikmal Hakem A Aziz
    ;
    Noorina Hidayu Jamil
    ;
    Laila Mardiah Deraman
    Currently, novel inorganic alumino-silicate materials, known as geopolymer composites, have emerged swiftly as an ecobenevolent alternative to contemporary ordinary Portland cement (OPC) building materials since they display superior physical and chemical attributes with a diverse range of possible potential applications. The said innovative geopolymer technology necessitates less energy and low carbon footprints as compared to OPC-based materials because of the incorporation of wastes and/or industrial byproducts as binders replacing OPC. The key constituents of ceramic are silica and alumina and, hence, have the potential to be employed as an aggregate to manufacture ceramic geopolymer concrete. The present manuscript presents a review of the performance of geopolymer composites incorporated with ceramic waste, concerning workability, strength, durability, and elevated resistance evaluation.
  • Publication
    Modern materials – obtaining and characterization (alloys, polymers)
    ( 2021)
    Bogusław Major
    ;
    Andrei Victor Sandu
    ;
    Mohd. Mustafa Al Bakri Abdullah
    ;
    Marcin Nabiałek
    ;
    Tomasz Tański
    ;
    Adam Zieliński
  • Publication
    The effect of particle size on the mechanical properties of Alkali Activated Steel Slag Mortar
    ( 2022)
    Doh Shu Ing
    ;
    Ho Chia Min
    ;
    Xiaofeng Li
    ;
    Ramadhansyah Putra Jaya
    ;
    Mohd. Mustafa Al Bakri Abdullah
    ;
    Siew Choo Chin
    ;
    Nur Liza Rahim
    ;
    Marcin Nabiałek
    With the rapid development of industry, abundant industrial waste has resulted in escalating environmental issue. Steel slag is the by-product of steel-making and can be used as cementitious materials in construction. However, the low activity of steel slag limits its utilization. Much investigation has been conducted on steel slag, while only a fraction of the investigation focuses on the effect of steel slag particle size on the properties of mortar. The aim of this study is to investigate the effect of steel slag particle size as cement replacement on properties of steel slag mortar activated by sodium sulphate (Na 2 SO 4). In this study, two types of steel slag, classified as fine steel slag (FSS) with particle sizes of 0.075mm and coarse steel slag (CSS) with particle sizes of 0.150 mm, were used for making alkali activated steel slag (AASS) mortar. Flow table test, compressive strength test, flexural strength test and UPV test were carried out by designing and producing AASS mortar cubes of (50 × 50 × 50) mm at 0, 10%, 20% and 30% replacement ratio and at 0.85% addition of Na 2 SO 4. The results show that the AASS mortar with FSS possess a relatively good strength in AASS mortar. AASS mortar with FSS which is relatively finer shows a higher compressive strength than CSS up to 38.0% with replacement 52 DOH SHU ING et al. ratio from 10% to 30%. This study provided the further investigation on the combined influence of replacement ratio and particle size of SS in the properties of fresh and hardened AASS.