Lee Chang Chuan
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Lee Chang Chuan
Official Name
Lee, Chang Chuan
Alternative Name
Lee, Cc
Chuan, Lee Chang
Lee, C. C.
Chuan, Lee C.
Lee, Chang Chuan
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Scopus Author ID
55312531900

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  • Publication
    Microwave synthesis of silicon carbide nanowhiskers: Effect of molar ratio
    ( 2020-01-01)
    Lee Chang Chuan
    ;
    Kahar S.M.
    ;
    Voon Chun Hong
    Silicon carbide (SiC) is an attractive material for its excellent properties such as wide band gap, high chemical stability and thermal conductivity. The conventional methods for the preparation of SiC are time and energy consuming. In this paper, SiC nanowhiskers were synthesized by utilizing microwave heating. Mixture of graphite and silica of various ratio was heated to 1400 °C for 30 min at a heating rate of 20 °C/min. It was found that almost complete conversion of graphite and silica to silicon carbide nanowhiskers was observed for sample of mixture in the ratio of 1:3. Vapor-solid mechanism was suggested to explain the formation of SiC nanowhiskers.
  • Publication
    Effective synthesis of silicon carbide nanotubes by microwave heating of blended silicon dioxide and multi-walled carbon nanotube
    ( 2017)
    Voo Chung Sung Tony
    ;
    Voon Chun Hong
    ;
    Lee Chang Chuan
    ;
    Lim Bee Ying
    ;
    Subash Chandra Bose Gopinath
    ;
    Foo Kai Loong
    ;
    Mohd Khairuddin Md Arshad
    ;
    Ruslinda A. Rahim
    ;
    Uda Hashim
    ;
    Nashaain Mohd Nordin
    ;
    Yarub Al-Douri
    Silicon carbide nanotube (SiCNTs) has been proven as a suitable material for wide applications in high power, elevated temperature and harsh environment. For the first time, we reported in this article an effective synthesis of SiCNTs by microwave heating of SiO2 and MWCNTs in molar ratio of 1:1, 1:3, 1:5 and 1:7. Blend of SiO2 and MWCNTs in the molar ratio of 1:3 was proven to be the most suitable for the high yield synthesis of β-SiCNTs as confirmed by X-ray diffraction pattern. Only SiCNTs were observed from the blend of MWCNTs and SiO2 in the molar ratio of 1:3 from field emission scanning electron microscopy imaging. High magnification transmission electron microscopy showed that tubular structure of MWCNT was preserved with the inter-planar spacing of 0.25 nm. Absorption bands of Si-C bond were detected at 803 cm-1 in Fourier transform infrared spectrum. Thermal gravimetric analysis revealed that SiCNTs from ratio of 1:3 showed the lowest weight loss. Thus, our synthetic process indicates high yield conversion of SiO2 and MWCNTs to SiCNTs was achieved for blend of SiO2 and MWCNTs in molar ratio of 1:3.
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