Khairul Anwar Abdul Halim
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Preferred name
Khairul Anwar Abdul Halim
Official Name
Abdul Halim, Khairul Anwar
Alternative Name
Halim, Khairul Anwar Abdul
Halim, Khairul Anwar A.
A. Halim, Khairul Anwar
Halim, K. A.Abdul
Anwar Abdul Halim, Khairul
Main Affiliation
Scopus Author ID
57197793640
Researcher ID
AAH-3722-2021

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  • Publication
    The effect of various nanoclay surface modifications on the thermal and mechanical properties of amorphous polyamide nanocomposites
    ( 2020-01-01)
    Khairul Anwar Abdul Halim
    ;
    Kennedy J.E.
    ;
    Farrell J.B.
    ;
    Muhammad Salihin Zakaria
    The addition of nanoclay within polymer matrix is anticipate to enhance the properties of the polymer system. Nonetheless, one of the key elements in property enhancements of a polymer nanocomposites is the surface modifications of the nanoclay. This is due to the affinity between polymer matrix and nanoclay is of important factors should be considered. In this study, amorphous polyamide was melt blended with different nanoclay grades with different surface modifications in order to evaluate the best clay grade for the polymer system. The thermal analysis carried out on the amorphous polyamide nanocomposites were carried out by means of differential scanning calorimetry (DSC) and dynamic mechanical analysis (DMA) whereas the mechanical properties were investigated using tensile testing. It was observed that there were changes in the glass transition temperature (Tg) of the nanocomposites due to clay additions. Further, the storage modulus was found to increase as a result of nanoclay incorporation. The type of clay grades significantly affects the mechanical properties of the amorphous polyamide nanocomposites.
  • Publication
    The effect of synthesis parameter On HKUST-1 nanocomposites studied by FTIR characterisation and mechanical testing
    ( 2024-12)
    Syazwana Ahmad
    ;
    Mohd Firdaus Omar
    ;
    Khairul Anwar Abdul Halim
    ;
    Shayfull Zamree Abd. Rahim
    ;
    Sam Sung Ting
    ;
    E. M. Mahdi
    ;
    Hazizan Md Akil
    ;
    Muhammad Hafiz Hassan
    ;
    Norlin Nosbi
    ;
    Nurfina Yudasari
    In the present work, Hong Kong University of Science and Technology (HKUST-1) has been synthesised at room temperature with 1:0, 1:1 and 0:1 ratio of ethanol and water and reinforced into polyurethane. In order to understand the impact of synthesis parameters on HKUST-1 nanocomposites, an investigation was conducted using FTIR characterisation and mechanical testing. The objective was to examine the potential improvement of the reinforced polymer. The mechanical testing results were shown to be significantly influenced by the presence of HKUST-1 with 1:0 ratio of ethanol and water (sample A) into polyurethane (PU). The samples underwent Fourier Transform Infrared Spectroscopy (FTIR) analysis to determine the types of bonds within the polymer-MOF nanocomposites. It was observed that the reinforced nanoparticles did not undergo any chemical changes, as indicated by the recorded spectra, which can be related to the overlapping characteristics of HKUST-1 and PU. The findings indicate that the A/PU exhibited a notable impact in comparison to other materials, as evidenced by the results of the tensile test and nanoindentation study.
  • Publication
    A Review: Polymer-based Insulation Material for HVDC Cable Application
    ( 2020-12-18)
    Syatirah Mohd Noor
    ;
    Muhamad N.A.
    ;
    Khairul Anwar Abdul Halim
    ;
    Mohamad Zhafran Zakariya
    ;
    Anuar, Muhammad Nuqman K.
    ;
    Aimi Athirah Hazwani Zaidi
    Demand on the usage of HVDC cables in the past was very low, this is because at that time most its application is only for underwater cable installations. However, when there are an increased in demand for using renewable energy such as solar energy, the use of polymer-based as insulaton material for HVDC became increased. This have attracted more cable manufacturers try to improve this cable quality and attract more market penetration in order make the development costs recoverable. This paper presents a review the used of polymer-based material for HVDC cable application. Comparison and discussion from previous researcher and manufacturer was done in term of material properties and quality was presented and discussed. The review was focused 4 types of polymer-based material which are: cross-linked Polyethylene (XLPE), low-density polyethylene (LDPE), high-density polyethylene (HDPE), linear low-density polyethylene (LLDPE). Each material tests result were discussed for the best usage as HVDC insulation systems. The review found, polymer based material with additional of nana filler or difference type polymer can improve dielectric properties of HVDC cable insulator. This is because these material have very good indication of the conductivity and dielectric strength of high voltage insulation for HVDC application.
  • Publication
    The Effects of Epoxidised Natural Rubber (ENR-50) on Cure Characteristics and Tensile Properties of Recycled Natural Rubber Catheter Filled Ethylene Propylene Diene Monomer (EPDM) Vulcanizates
    ( 2020-11-24)
    Muhammad Salihin Zakaria
    ;
    Nik Noriman Zulkepli
    ;
    Nordin R.M.
    ;
    Khairul Anwar Abdul Halim
    ;
    Hanafi H.
    The effect of epoxidised natural rubber (ENR-50) on cure characteristics and tensile properties (tensile strength, modulus at 100% elongation and elongation at break) of recycled natural rubber catheter filled ethylene propylene diene monomer (EPDM) vulcanizates were studied. The scorch time, t2 of EPDM/NRr blends with and without ENR-50 increased as NRr content increased while the cure time, t90 is decreased. However, with the presence of ENR-50 in EPDM/NRr blends, the t2 was longer and t90 was shorter than the uncompatibilized EPDM/NRr blends. The minimum torque, ML, of EPDM/NRr blend with and without ENR-50 relatively increased while maximum torque, MH, decreased with increasing NRr content. With the presence of ENR-50, the compatibilized EPDM/NRr blends exhibit a lower value of ML and MH compared with uncompatibilized blends. The incorporation of ENR-50 in EPDM/NRr blends enhanced the tensile strength and tensile modulus of compatibilized EPDM/NRr blends compared to uncompatibilized EPDM/NRr blends. The elongation at break (Eb) of compatibilized EPDM/NRr blends is lower than the uncompatibilized EPDM/NRr blends at all blend ratios. This indicated that ENR 50 improved the curing characteristics and tensile properties of the compound.
  • Publication
    Effect of Al2O3 Nanofillers on Polarization and Depolarization Current (PDC) of New LLDPE/HDPE Compounding for HVDC Application
    ( 2022-01-01)
    Noor S.M.
    ;
    Muhamad N.A.
    ;
    Khairul Anwar Abdul Halim
    ;
    Ghani S.A.
    ;
    Darussalam B.
    ;
    Mohd Jamil M.K.
    Polymeric nanocomposites are being used more frequently to replace traditional insulation because they offer superior mechanical and electrical qualities. An efficient and successful diagnostic method based on time domain measurement is Polarization and Depolarization Current (PDC) measurement, which tracks the behaviour of the dielectric. Finding novel materials with improved dielectric properties is one of the key goals of research in the field of polymer nanocomposite dielectrics. This study uses the Polarization and Depolarization Current (PDC) measuring technique to examine the conductivity variation of LLDPE nanocomposite for formulations of HDPE blends nanocomposites made from polyethylene filled with nanoparticles of Al2O3. The goal of the experiment was to determine each sample's individual conductivity fluctuations and PDC pattern. The optimal composition for HV insulation in terms of lowest polarization and depolarization current values and lowest conductivity was discovered to be LLDPE/HDPE- Al2O3at 5%wt of nanofiller. The findings indicate that adding a certain amount of nanofiller to LLDPE/HDPE-based materials improved the materials' dielectric strength.
  • Publication
    Short review: biowaste as a source of silica and Its application as a filler to fabricate the superhydrophobic silica-based coating
    ( 2024-03)
    Nur Fatihah Mohd Fadzil
    ;
    Muhammad Salihin Zakaria
    ;
    Khairul Anwar Abdul Halim
    ;
    Nur Farhana Hayazi
    ;
    Lokman Hakim Ibrahim
    ;
    Razif Muhammed Nordin
    Silica (SiO2) plays a major key ingredient in producing products such as toothpaste, ceramics, and paints, to name a few, as it acts as a stabilizing agent, filler and additive. Due to its excellent properties, the use of high-purity SiO2 in industrial applications is favourable. Unfortunately, high-purity SiO2 is expensive. Tetraethyl Orthosilicate (TEOS) is an example of a SiO2 precursor that is costly and harmful, yet frequently employed. This paper provides a short review of the advantages of biowaste materials as SiO2 precursors and their role as fillers in the fabrication of superhydrophobic coating. Researchers nowadays are attempting to lower the expense of employing high-purity SiO2 by extracting silica from biowaste using many methods such as acid leaching and alkali treatment as this option is highly sustainable. The growth of agricultural industries is exponential due to the increase in biowaste production. Therefore, this is one of the ways to utilize the use of biowaste in combatting the environmental issues regarding excess biowaste and receding pure resources. SiO2 from biowaste also can be utilized as filler and used to develop superhydrophobic coating, providing numerous potential applications.
  • Publication
    Sugarcane Bagasse Reinforced Polyester Composites: Effects of Fiber Surface Treatment and Fiber Loading on the Tensile and Flexural Properties
    ( 2020-11-24)
    Muhammad Salihin Zakaria
    ;
    Luqman Musa
    ;
    Nordin R.M.
    ;
    Khairul Anwar Abdul Halim
    The effect of fiber surface treatment and fiber loading on the tensile and flexural properties of untreated and treated fiber-based sugarcane bagasse reinforced polyester (SBRP) composites have been investigated. Sugarcane bagasse fibers were alkalized with 1, 3 and 5% concentration of sodium hydroxide (NaOH) solution combined with different fiber loading formulation 0, 20, 30 and 40 php, and hot-pressed to form natural fibers composite were prepared. The results indicated that the incorporation of bagasse fiber composites alkalized with 3% NaOH solution improved the tensile strength and modulus of reinforced composites meanwhile the untreated bagasse gave the lowest value. However, the elongation at break (Eb) indicated that treated bagasse fiber composites show a lower value compared to untreated composites. A similar trend also obtained for flexural strength and modulus.
  • Publication
    Influence of sodium chloride on recycled HDPE in superhydrophobic surface development
    ( 2024-12)
    Thor Keat Seng
    ;
    Muhammad Salihin Zakaria
    ;
    Razif Muhammed Nordin
    ;
    Khairul Anwar Abdul Halim
    ;
    Nur Farhana Hayazi
    ;
    Lokman Hakim Ibrahim
    Inspired by lotus leaf, superhydrophobic surfaces have emerged rapidly in recent years. It is due to its excellence ability in self-cleaning and corrosion protection, to name a few. In this research, a green superhydrophobic surface was constructed on the surface of recycled High-Density Polyethylene (rHDPE) by utilizing Sodium chloride (NaCl) as a water-soluble surface modifying agent. The treatment process is simple,and cost-efficient as it only used rHDPE and NaCl as the main materials with additional chemicals and at the same time leave no impact on the environment. Variation of NaCl grinding period influenced the value of CA by which 240 minutes grinded NaCl displayed highest CA of 161.4°. This may be attributed by the increase of surface roughness as the grinding time increase. Furthermore, the surface morphology, topography, and self-cleaning ability of superhydrophobic surafce were analyzed to further understand the surface characteristics. The anti-sticking and self-cleaning properties were successfully displayed by the superhydrophobic surface thus, showing its potential as an eco-friendly material.
  • Publication
    The effect of twin screw compounding parameters on the tensile properties of pineapple leaf/sea shell hybrid polymer composite using DOE approach
    ( 2020-11-24)
    Ching N.T.
    ;
    Khairul Anwar Abdul Halim
    ;
    Mohd Firdaus Omar
    ;
    Azlin Fazlina Osman
    ;
    Muhammad Salihin Zakaria
    Pineapple leaf and sea shell were used as natural fillers in this research due to its biodegradable nature, wide availability, continuous resources and low cost. This research work was carried out to investigate the effect of compounding process using twin screw extruder on the tensile performance of pineapple leaf / sea shell polymer composite using Design of Experiment (DOE) approach. A total of nine runs of were formulated and the resulitng hybrid composites were compounded using twin screw extruder. The short term tensile test was carried out to determine the tensile properties and the data were sunsequently analyse using DOE software. Pareto chart of the standardized effect and the main effect plot were employed to investigate the relationship between processing parameters and the tensile performance of the hybrid composite systems. Based on the initial DOE analysis, it is shown that compounding parameters had influenced the final mechanical behavior of the hybrid composites.
  • Publication
    The use of ground & ultrasonicated dolomite (GUD) for improving the tensile performance of Poly (ethylene-co-vinyl acetate) copolymer composite
    ( 2021-11-12)
    Fauzi A.A.A.
    ;
    Azlin Fazlina Osman
    ;
    Khairul Anwar Abdul Halim
    ;
    Mustafa Z.
    ;
    Alakrach A.M.
    ;
    Mohd Nazry Salleh
    The combination of the organic and inorganic materials to fabricate a new form of material called 'composite' has been performed since several decades ago. However, the strategy to improve the homogeneity of the resultant composite system is still being the main focus of current research. In this study, dolomite and poly (ethylene-co-vinyl acetate) (PEVAc) were employed as filler and matrix, respectively. Dolomite was ground and ultrasonicated before being used as filler. It can be observed that the size of dolomite particles has been reduced significantly upon the grinding and ultrasonication processes. The effect of ground and ultrasonicated dolomite (GUD) addition on the mechanical performance of the PEVAc copolymer was investigated. Results indicate that the GUD filler has successfully increased the tensile strength, elongation at break, modulus of elasticity and tensile toughness of the PEVAc copolymer when being employed in 1 wt%. However, the use of higher content of GUD resulted in the decreasing trend of those properties. This shows that the ground and ultrasonicated dolomite with smaller and higher surface area particles than its pristine form could bring improvement to the mechanical performance of the copolymer when being used in low loading as it can be more easily dispersed in the copolymer matrix.