Now showing 1 - 10 of 11
  • Publication
    Interaction of Geopolymer Filler and Alkali Molarity Concentration towards the Fire Properties of Glass-Reinforced Epoxy Composites Fabricated Using Filament Winding Technique
    This paper aims to find out the effect of different weight percentages of geopolymer filler in glass-reinforced epoxy pipe, and which can achieve the best mechanical properties and adhesion between high calcium pozzolanic-based geopolymer matrices. Different weight percentages and molarities of epoxy hardener resin and high calcium pozzolanic-based geopolymer were injected into the glass fiber. By manually winding filaments, composite samples were produced, and they were then allowed to cure at room temperature. To determine how well the geopolymer matrices adhere to the fiber reinforcement, the microstructure of the composites’ surfaces and perpendicular sections were examined. Maximum values of compressive strength and compressive modulus were 94.64 MPa and 2373.58 MPa, respectively, for the sample with a weight percentage of filler loading of 30 wt% for an alkali concentration of 12 M. This is a relatively wide range of geopolymer weight percentage of filler loading from 10 wt% to 40 wt%, at which we can obtain high compressive properties. By referring to microstructural analysis, adhesion, and interaction of the geopolymer matrix to glass fiber, it shows that the filler is well-dispersed and embedded at the fiber glass, and it was difficult to determine the differences within the range of optimal geopolymer filler content. By determining the optimum weight percent of 30 wt% of geopolymer filler and microstructural analysis, the maximum parameter has been achieved via analysis of high calcium pozzolanic-based geopolymer filler. Fire or elevated temperature represents one of the extreme ambient conditions that any structure may be exposed to during its service life. The heat resistance or thermal analysis between glass-reinforced epoxy (GRE) pipe and glass-reinforced epoxy pipe filled with high calcium pozzolanic-based geopolymer filler was studied by investigating burning tests on the samples, which shows that the addition of high calcium pozzolanic-based geopolymer filler results in a significant reduction of the melted epoxy.
      1
  • Publication
    Interaction of geopolymer filler and alkali molarity concentration towards the fire properties of glass-reinforced epoxy composites fabricated using filament winding technique
    This paper aims to find out the effect of different weight percentages of geopolymer filler in glass-reinforced epoxy pipe, and which can achieve the best mechanical properties and adhesion between high calcium pozzolanic-based geopolymer matrices. Different weight percentages and molarities of epoxy hardener resin and high calcium pozzolanic-based geopolymer were injected into the glass fiber. By manually winding filaments, composite samples were produced, and they were then allowed to cure at room temperature. To determine how well the geopolymer matrices adhere to the fiber reinforcement, the microstructure of the composites’ surfaces and perpendicular sections were examined. Maximum values of compressive strength and compressive modulus were 94.64 MPa and 2373.58 MPa, respectively, for the sample with a weight percentage of filler loading of 30 wt% for an alkali concentration of 12 M. This is a relatively wide range of geopolymer weight percentage of filler loading from 10 wt% to 40 wt%, at which we can obtain high compressive properties. By referring to microstructural analysis, adhesion, and interaction of the geopolymer matrix to glass fiber, it shows that the filler is well-dispersed and embedded at the fiber glass, and it was difficult to determine the differences within the range of optimal geopolymer filler content. By determining the optimum weight percent of 30 wt% of geopolymer filler and microstructural analysis, the maximum parameter has been achieved via analysis of high calcium pozzolanic-based geopolymer filler. Fire or elevated temperature represents one of the extreme ambient conditions that any structure may be exposed to during its service life. The heat resistance or thermal analysis between glass-reinforced epoxy (GRE) pipe and glass-reinforced epoxy pipe filled with high calcium pozzolanic-based geopolymer filler was studied by investigating burning tests on the samples, which shows that the addition of high calcium pozzolanic-based geopolymer filler results in a significant reduction of the melted epoxy.
      6  27
  • Publication
    Effect of winding speed in epoxy glass composites for new fabricated filament winding machin
    The production of the glass fiber reinforced epoxy pipes is produced by filament winding process due to of its low costs, convenient and easy to install. The main objectives of this research is to optimize new fabricated filament winding machine and investigate the effect of winding speed. The problems for a new fabricated filament winding machine that must be optimized at first and lack of data for parameter in winding speed. The production by using filament winding process can be produce varieties of products such as tanks, pipes and vessels. The production of glass reinforced epoxy pipes of filament winding process was used different of winding speed levels. The new fabricated filament winding machine have 6 different winding speed that must be tested to get the optimum mechanical strength results. The process was stopped when the thickness of the samples is about 5.5mm wall thickness. The samples were tested with density for physical test and compressive strength for mechanical testing. The optimum winding speed to produce high mechanical strength for this new fabricated filament winding machine is winding speed two and the angle of the winding for speed 2 is 55°. This study, helps to determine winding speed for calibrate new filament winding.
      6  30
  • Publication
    Mechanical Effect on Different Geopolymer Filler in Glass Reinforced Epoxy Composite
    Glass reinforced epoxy are widely known in oil and gas industry as glass reinforced epoxy pipe. However, glass reinforced epoxy has limitation such as demanding careful handling due fabrication, installation and transportation because of brittle nature itself and low compressive strength. The aim of this research is to characterize and study the effect of different geopolymer filler in the glass reinforced epoxy pipe composites. Filament winding method will be used in producing glass reinforced epoxy composite. Samples will be prepared with different weight percentage of geopolymer filler loading and different types of geopolymer filler which is fly ash-based geopolymer and kaolin-based geopolymer with 10wt% - 40wt% of geopolymer filler loading. Microstructure was obtained by using Scanning Electron Microscopy showed spherical shaped of fly ash raw material and plate-like structure for kaolin raw material. After undergoes the mechanical testing involved compressive test, pipe sample of glass reinforced epoxy filled with 20 wt% of fly ash-based geopolymer filler showed the best performances above them all. The compressive strength value was 43.05 MPa. Glass reinforced epoxy composite pipe filled with different geopolymer are not widely used in this research area. Therefore, by using geopolymer as a filler can improve the properties of glass reinforced epoxy composite pipe. Hence, a waste material like geopolymer can reduce the cost of material and improve the environment.
      1
  • Publication
    Effects of Different Fiber Sizes in PLA/Carbon Fiber Composites on Mechanical Properties
    This study assessed the morphology and chemical composition of coir coconut husk carbon fiber, as well as the impact of fiber diameters on the physical and mechanical properties of polylactic acid composites. Researchers are studying polylactide acid, a biodegradable material. This eco-friendly material’s excellent features, generated from sustainable and renewable sources, have drawn many people. Malaysia’s high coconut fiber output made coir husk a popular commodity. Coconut fibers are lignin, cellulose, and hemicellulose. Alkaline treatment eliminates hemicellulose, oil, wax, and other contaminants from coir fibers and removes lignin. Fourier Transform Infrared Spectroscopy and Scanning Electron Microscopy were used to examine the treated coconut fibers’ chemical modification analysis and morphology. Coconut coir husk was carbonized to produce carbon fiber using a furnace operated at 300°C for 2 hours. Fiber and polylactic acid were mixed in different fiber sizes (0, 53 µm, 75 µm, and 212 µm) via extrusion and injection processing techniques. The results showed that the alkali treatment reduced the hydroxyl (-OH) group and separated the area from the carbonyl (C=O) group of coconut coir husk, which changed the filler’s hydrophilicity. The fiber size of 212 µm was discovered to have the highest tensile and flexural strength values. According to testing, the modified material structure had a better surface fill-matrix bond. Thus, generalized fiber sizing and characterization methods were developed. Regardless of the matrix, this method can characterize natural fiber strength and interfacial shear strength of varied diameters and solid contents.
      1  39
  • Publication
    EFFECT OF COMPOSITION ON MELT FLOW AND DENSITY OF POLYPROPYLENE COPOLYMER/KAOLIN GEO-FILLER COMPOSITES
    ( 2023-01-01)
    Zulkifli Z.
    ;
    ; ; ;
    Aygörmez Y.
    This study examined the effects rheological properties of different composition kaolin and kaolin geo-filler in polypropylene composites. Polypropylene composites with varying composition of kaolin geo-filler 0 wt%, 2 wt%, 4 wt%, 6 wt%, 8 wt%, and 10 wt% was prepared and compared with polypropylene composite with raw kaolin. Kaolin is an aluminosilicate based mineral filler was used to prepare geopolymer paste by combining with alkaline activator solution. The polypropylene composite was compounded using a twin-screw extruder and the melt flow index was determined by a constant weight pressure of 2.16 kg at 230°C in 10 min. Knowing the melt flow index is necessary to predict and control the process, the study has demonstrated that the composition of kaolin filler and kaolin geo-filler affects the melt flow, melt density and surface morphology at varies composition. Composites with kaolin geo-filler have demonstrated high melt flow index process and having better distribution and flow.
      4  28
  • Publication
    Mechanical effects on different solid to liquid ratio of geopolymer filler in epoxy resin
    Geopolymer is formed from the alkali activation of materials rich in Si and Al content with the addition of a silicate solution to enhance the properties of the materials. This paper presents research on the mechanical properties of fly ash-based geopolymer filler in epoxy resin by varying different solid to liquid ratios using sodium hydroxide and sodium silicate as the alkaline activator. However, the common problem observed from the solid to liquid ratio is the influence of curing time and compressive strength of geopolymer to have the best mechanical property. The mix design for geopolymers of solid to liquid ratio is essential in developing the geopolymer’s mechanical strength. A series of epoxy filled with fly ash-based geopolymer materials with different solid to liquid ratio, which is prepared from 0.5 to 2.5 solid to liquid ratio of alkaline activator. The tensile strength and flexural strength of the epoxy filled with fly ash-based geopolymer materials is determined using Universal Testing Machine under tensile and flexural mode. It was found that the optimum solid to liquid ratio is 2.0, with the optimum tensile and flexural strength value. However, both the tensile and flexural properties of epoxy filled with fly ash-based geopolymer suddenly decrease at a 2.5 solid to liquid ratio. The strength is increasing with the increasing solid to liquid ratio sample of geopolymer filler content.
      6  20
  • Publication
    Corrosion Control by Using Aluminium as Sacrificial Anode Cathodic Protection (SACP) in Geopolymer Reinforced Concrete
    This paper presents corrosion control by using Aluminium as Sacrificial Anode Cathodic Protection (SACP) in geopolymer reinforced concrete. Geopolymer concrete for this research are the combination and reaction between kaolin, which is acting as a binder, fine aggregates such as river sand, coarse aggregates and an alkaline activator which contain 12 M of sodium hydroxide (NaOH) solution and sodium silicate (Na2SiO3) solution with the ratio of NaOH/Na2SiO3 is 0.8. There are two types of sample preparation in this experiment which are the control sample without attaching with Aluminium and SACP sample that attach to Aluminium. Three testing were conducted in this research such as compressive strength, open circuit potential and gravimetric weight loss method and these results were observed after days 7 and 14. Compressive strength testing for this geopolymer concrete shows that the highest compressive strength was at sample 14 days which is 7.04 MPa while sample 7 days is 3.96 MPa. The result shows the potential values of SACP samples were lower than the control sample for both 7 and 14 days. The potential values for the SACP sample for 7 and 14 days are 0.0152 V and -0.037 V while for control sample was 0.048 V and 0.051 V respectively. From the Pourbaix diagram, the control sample was located in the passivity region while SACP sample was located in the immunity region. The corrosion rate of the reinforcement bar in concrete has been performed by the gravimetric weight loss method. Analysis of the resulting proved that the corrosion rate of SACP sample was lower than the control sample for both 7 and 14 days, which were 3.60 x 10-5 mm/yr and 1.427 x 10-5 mm/yr respectively. This is due to the presence of Aluminium which act as the sacrificial anode that protects reinforcement bar in geopolymer concrete from the corrosive agent.
      3  36
  • Publication
    Flexural properties of polyethylene composites based kaolin geo-filler
    ( 2020-11-02) ;
    Shern Tan Wei
    ;
    ; ;
    Lun Loh Zhen
    ;
    Hasri
    ;
    Hartati
    Polyethylene has wide applications as a single matrix, however it has a weakness such as low mechanical properties. Kaolin is based mineral filler that offered mechanical performance, it has been used as a cost-effective reinforcing filler for many thermoplastic materials. However, the incorporation of kaolin into thermoplastic often requires the use of compatibilizer or surface treatment to increase the mechanical performance of the composites. In this study, kaolin has been utilized as geo-filler through geopolymerization process by alkaline solution to increase the interfacial adhesion of materials in the composite. Kaolin geo-filler was found having compact structure and to improve the mechanical properties at lower filler loading. Flexural test according to ASTM D790 was performed whereas Scanning Electron Microscopy was used to observe the fracture surface. The testing and micrography are compared with the properties of raw kaolin filler on polyethylene composite. The results found that 8 % of kaolin geo-filler content is optimal for polyethylene composite and show better flexural properties.
      5  24
  • Publication
    Tensile Properties of Polyethylene Composites Based Kaolin Geo-Filler
    The current work studies the tensile properties of polyethylene composites-based kaolin geo-filler. Polyethylene composites was prepared based on kaolin geo-filler at different loading content varies from 0,2,4,6,8 and 10 wt%. The optimum results were compared with polyethylene composites based on raw kaolin to study the effect both filler on tensile properties. Tensile test was conducted according to ASTM D638. Based on these research studies, the use of kaolin geo-filler is effectively improved the tensile properties of polyethylene as compared to the raw kaolin filler. As the result, 8% of kaolin geo-filler content demonstrate the optimum formulation to enhance the tensile properties of polyethylene composites.
      6  39