Research Output
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PublicationPreliminary study of the polymesoda expansa based hydroxyapatite for medical devices coating application( 2020-12-15)Hydroxyapatite (HA) which is a group of calcium phosphate (CaP) is used as a medical devices coating due to its ability to increase the bioactivity and biocompatibility of the device surface. The attraction of using waste seashells products is interesting due to its sustainability and low cost solution especially in biomedical application. Polymesoda expansa or locally known as Lokan is potentially rich with calcium carbonate (CaCO3). Here, the synthesis of HA was done via precipitation method by utilizing the Polymesoda expansa (Lokan) shells as the resource of calcium precursors. Hydroxyapatite synthesized from Polymesoda expansa was carried out with different pH solution (pH 9 and 13) in alkaline environment. The effects of pH on the morphological and chemical composition properties as well as the Ca/P ratio of HA powders were analyzed through Scanning Electron Microscopy (SEM), Fourier Transform Infrared Spectroscopy (FTIR), and Energy Dispersive X-ray Spectrometry (EDS). The finding demonstrates as the pH increases, the calcium apatite reduced and this had increases the Ca/P ratio.
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PublicationNano Hydroxyapatite (Nano-HA) based on pholas orientalis shells and degradation analysis( 2023-04)Millions of tons of seashells are produced every day as waste around the world. These underutilized seashells waste was executed as calcium precursor by researcher to synthesis the nano-hydroxyapatite (nano-HA). Nano-HA was successfully synthesised from Pholas Orientalis seashells waste via the chemical precipitation method. Different sintering temperatures were implemented to evaluate the physicochemical criteria of nano-HA. The obtained powders were examined by various physicochemical methods such as XRD, FTIR, FESEM, EDX and degradation analysis. The peaks in XRD and FTIR analysis the HA is successfully produced. The FESEM images on the other hand showing the HA particle in nano size range with rice-like structure. Meanwhile, a variation of Ca/P ratio can be observed in respect to sintering temperatures. The Ca/P ratio for HA-WS, HA-S500 and HA-S700 sample is 1.78, 2.03 and 1.57 respectively. Different sintering temperatures result in different crystallinity value which consequently affects its degradation profile.
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PublicationSynthesizing and Optimization the Hydroxyapatite Based on Corbiculacea Seashells( 2021-01-01)Hydroxyapatite (HA) is one of the main components in bone which functions to enhance its cell regeneration. Synthetically produced HA, based on seashell resources has higher biocompatibility, and in high demand especially in bone tissue engineering. However, the secondary phase of HA production are calcium oxide and carbonate, which impedes its performance. HA is synthesized via wet chemical precipitation and optimization were done to obtain nearly pure HA by manipulating the pH value and sintering temperature. It is expected that the combination of these parameters will optimize the amount of secondary phase hence attained nearly stoichiometric or pure HA. HA powders were analyzed through Fourier Transform Infrared Spectroscopy (FTIR) and Energy Dispersive X-ray Spectrometry (EDX).
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