The mechanical and morphological properties of PVOH/kenaf fibre thin film was studied. The additive used on this research was tapioca starch. Thin films were fabricated using method of solution casting. The thin films composites with different kenaf fibre loadings (0, 5, 10, 15, 20, 30 wt%) were mixed at a temperature of 80 °C with water bath for 1 h and casted on petri dish and let them oven dried at 50 °C for 24 h. The purpose of the current research was to determine the mechanical and morphological properties of PVOH/KF thin film composites with and without addition of starch. The results of this investigation show that the thin film with addition of 5 wt% of tapioca starch has better tensile strength, which is 35.15 MPa, compare to without tapioca starch, which is 29 MPa. The second major finding was that the morphological observed using scanning electron microscope (SEM) reveals improvement of adhesion between kenaf fibre with PVOH matric as addition of tapioca starch.
