This study focuses on the synthesis of synthetic calcium monosilicate ceramic from chicken eggshells and rice husks waste through the mechanochemical route that relatively straightforward without adding any binders. Synthetic calcium monosilicate was mixed using a 1:1 ratio of calcined eggshell and rice husk ash, which both materials known as rich in calcium oxide and silica sources, respectively. The mixed powder was pressed using uniaxial pressing before fired at 1100oC, 1150oC, 1200oC, 1250oC, and 1300oC for 120 minutes with a heating rate of 5oC/min. The XRD spectrum from 1100oC to 1200oC mainly consists of pseudowollastonite (ICSD: 98-005-2576), wollastonite and silicon dioxide phases. However, as the sintering temperature increases, the wollastonite phases was completely transformed into pseudowollastonite, leaving some unreacted silica.