LiV₃O₈ layered structure was successfully synthesized by a conventional solid-state approach and subsequent heat-treated at 400, 450, 500 and 550 ºC. The samples were characterized by XRD, SEM, TEM, BET. Electrochemical performance of LiV₃O₈ was investigated by cyclic voltammetry (CV) and galvanostatic charge-discharge. The results showed that high purity of LiV3O8 with layered structure was formed. The morphology of the samples were mixed between nanorods and nanosheets structure. For electrochemical performance, results showed that LiV₃O₈ heat-treated at 500 ºC performed a highest charge and discharge capacity of 212 and 172 mAh g-1, respectively. From electrochemical performance results made them a good candidate for cathode material for lithium-ion batteries application.
