Home
  • English
  • Čeština
  • Deutsch
  • Español
  • Français
  • Gàidhlig
  • Latviešu
  • Magyar
  • Nederlands
  • Português
  • Português do Brasil
  • Suomi
  • Log In
    New user? Click here to register. Have you forgotten your password?
Home
  • Browse Our Collections
  • Publications
  • Researchers
  • Research Data
  • Institutions
  • Statistics
    • English
    • Čeština
    • Deutsch
    • Español
    • Français
    • Gàidhlig
    • Latviešu
    • Magyar
    • Nederlands
    • Português
    • Português do Brasil
    • Suomi
    • Log In
      New user? Click here to register. Have you forgotten your password?
  1. Home
  2. Resources
  3. Journals
  4. International Journal of Nanoelectronics and Materials (IJNeaM)
  5. Synthesis of calcium phosphate: influence of sintering temperature on the formation of fluorhydroxyapatite
 
Options

Synthesis of calcium phosphate: influence of sintering temperature on the formation of fluorhydroxyapatite

Journal
International Journal of Nanoelectronics and Materials (IJNeaM)
ISSN
1985-5761
Date Issued
2020-01
Author(s)
Zudah Sima'atul Kubro
Bogor Agricultural University
Setyanto Tri Wahyudi
Bogor Agricultural University
Kiagus Dahlan
Bogor Agricultural University
Handle (URI)
https://ijneam.unimap.edu.my/
https://ijneam.unimap.edu.my/images/PDF/IJNEAM%20JAN%202020%20Vol%2013/Vol_13_No_1_2020_7_63-70.pdf
https://hdl.handle.net/20.500.14170/15334
Abstract
Calcium phosphate biomaterials can be classified as polycrystalline ceramics. Hydroxyapatite is one kind of calcium phosphate biomaterials which is also a mineral component in hard tissue, especially dental and bones. Hydroxyapatite has low chemical stability at high temperatures and low durability in an acidic environment. On the other hand, fluorhydroxyapatite has good chemical stability at high temperatures as well as the nature of its bioactivity. Fluorhydroxyapatite is made by adding F to replace some OH functional groups in hydroxyapatite. In this research, fluorhydroxyapatite was synthesized through precipitation method and microwave assistant with sintering temperatures of 600°C, 800°C, and 1000°C. Based on the characterization using an x-ray diffractometer, the results showed that at 1000°C sintering temperature, the samples have a higher intensity of fluorapatite and fewer impurities than other samples sintered at 800°C and 600°C. Fourier Transform Infra-Red (FTIR) analysis shows that similar functional groups appeared in the samples with all sintering temperatures. Conductivity evaluation shows that the conductivity values of the samples were inversely proportional to the sintering temperatures. The morphology of the samples not so clearly seen due to agglomeration, but it can be observed that fluorhydroxyapatite is flat-shaped needle-like or rod-shaped.
Subjects
  • Calcium phosphate

  • Fluorhydroxyapatite

  • Sintering temperature...

File(s)
Synthesis of Calcium Phosphate (1.05 MB)
google-scholar
Views
Downloads
  • About Us
  • Contact Us
  • Policies