Ceramics titanium silicon carbide Ti₃SiC₂ Max phase was rapidly synthesised and simultaneously consolidated by spark plasma sintering at which the extensive volume expansion occurred as a function of the temperature from ball milled SiC/Ti/C powders with Ti/SiC ratio of 3:1:2. The XRD patterns results were confirmed by FESEM observations and the EDAX analyses. The 3Ti+1.2SiC+0.8C nano-ceramics were processed from 3Ti+1.2SiC+0.8C/SWCNTs powders using spark plasma sintering (SPS) at temperatures of 1100, 1200 and 1300 oC with diting of SWCNTs from 0.0 to 1.0 wt% SWCNTs/Ti₃SiC₂ nanocomposite. The effects of SWCNTs addition on phases, microstructure and hardness of the nanocomposite were investigated. The best product contained 1.0 wt% CNTs/ Ti₃SiC₂/TiC which was sintered at 1300 °C, 60 MPa for 10 min The phase composition of the product could be tailored by adjusting the process parameters. The anisotropic hardness was observed in respect to the textured product.
