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Image analysis of surface porosity mortar containing processed spent bleaching earth

2021 , Beng Wei Chong , Rokiah Othman , Ramadhansyah Putra Jaya , Doh Shu Ing , Xiaofeng Li , Mohd Haziman Wan Ibrahim , Mohd. Mustafa Al Bakri Abdullah , Andrei Victor Sandu , Bartosz Płoszaj , Janusz Szmidla , Tomasz Stachowiak

Image analysis techniques are gaining popularity in the studies of civil engineering materials. However, the current established image analysis methods often require advanced machinery and strict image acquisition procedures which may be challenging in actual construction practices. In this study, we develop a simplified image analysis technique that uses images with only a digital camera and does not have a strict image acquisition regime. Mortar with 10%, 20%, 30%, and 40% pozzolanic material as cement replacement are prepared for the study. The properties of mortar are evaluated with flow table test, compressive strength test, water absorption test, and surface porosity based on the proposed image analysis technique. The experimental results show that mortar specimens with 20% processed spent bleaching earth (PSBE) achieve the highest 28-day compressive strength and lowest water absorption. The quantified image analysis results show accurate representation of mortar quality with 20% PSBE mortar having the lowest porosity. The regression analysis found strong correlations between all experimental data and the compressive strength. Hence, the developed technique is verified to be feasible as supplementary mortar properties for the study of mortar with pozzolanic material.

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Mechanical performance, microstructure, and porosity evolution of fly ash geopolymer after ten years of curing age

2023 , Ikmal Hakem A. Aziz , Mohd. Mustafa Al Bakri Abdullah , Rafiza Abd Razak , Zarina Yahya , Mohd Arif Anuar Mohd Salleh , Jitrin Chaiprapa , Catleya Rojviriya , Petrica Vizureanu , Andrei Victor Sandu , Muhammad Faheem Mohd. Tahir , Alida Abdullah , Liyana Jamaludin

This paper elucidates the mechanical performance, microstructure, and porosity evolution of fly ash geopolymer after 10 years of curing age. Given their wide range of applications, understanding the microstructure of geopolymers is critical for their long-term use. The outcome of fly ash geopolymer on mechanical performance and microstructural characteristics was compared between 28 days of curing (FA28D) and after 10 years of curing age (FA10Y) at similar mixing designs. The results of this work reveal that the FA10Y has a beneficial effect on strength development and denser microstructure compared to FA28D. The total porosity of FA10Y was also lower than FA28D due to the anorthite formation resulting in the compacted matrix. After 10 years of curing age, the 3D pore distribution showed a considerable decrease in the range of 5–30 µm with the formation of isolated and intergranular holes.

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Influence of salinity of mixing water towards physical and mechanical properties of high strength concrete

2023 , Rafiza Abd Razak , Khai Yen Ng , Mohd. Mustafa Al Bakri Abdullah , Zarina Yahya , M. Nabiałek , K. Muthusamy , W.A.W. Jusoh , B. Jeż , R. Mohamed

Dramatic population and economic growth result in increasing demand for concrete infrastructure, which leads to an increment of freshwater demand and a reduction of freshwater resources. However, freshwater is a finite resource, which means that freshwater will be used up someday in the future when freshwater demand keeps increasing while freshwater resources are limited. Therefore, replacing freshwater with seawater in concrete blending seems potentially beneficial for maintaining the freshwater resources as well as advantageous alternatives to the construction work near the sea. There have been few experimental research on the effect of blending water salt content on the mechanical and physical characteristics of concrete, particularly high-strength concrete. Therefore, a research study on the influence of salt concentration of blending water on the physical and mechanical properties of high-strength concrete is necessary. This study covered the blending water salinity, which varied from 17.5 g/L to 52.5 g/L and was determined on the physical and mechanical properties, including workability, density, compressive strength, and flexural strength. The test results indicate that the use of sea salt in blending water had a slight negative influence on both the workability and the density of high strength concrete. It also indicates that the use of sea salt in blending water had a positive influence on both the compressive strength and the flexural strength of high-strength concrete in an earlystage.

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Mechanical and durability analysis of fly ash based geopolymer with various compositions for rigid pavement applications

2022 , Muhammad Faheem Mohd. Tahir , Mohd. Mustafa Al Bakri Abdullah , Shayfull Zamree Abd. Rahim , Mohd Rosli Mohd Hasan , Andrei Victor Sandu , Petrica Vizureanu , Che Mohd Ruzaidi Ghazali , Aeslina Abdul Kadir

Ordinary Portland cement (OPC) is a conventional material used to construct rigid pavement that emits large amounts of carbon dioxide (CO2) during its manufacturing process, which is bad for the environment. It is also claimed that OPC is susceptible to acid attack, which increases the maintenance cost of rigid pavement. Therefore, a fly ash based geopolymer is proposed as a material for rigid pavement application as it releases lesser amounts of CO2 during the synthesis process and has higher acid resistance compared to OPC. This current study optimizes the formulation to produce fly ash based geopolymer with the highest compressive strength. In addition, the durability of fly ash based geopolymer concrete and OPC concrete in an acidic environment is also determined and compared. The results show that the optimum value of sodium hydroxide concentration, the ratio of sodium silicate to sodium hydroxide, and the ratio of solid-to-liquid for fly ash based geopolymer are 10 M, 2.0, and 2.5, respectively, with a maximum compressive strength of 47 MPa. The results also highlight that the durability of fly ash based geopolymer is higher than that of OPC concrete, indicating that fly ash based geopolymer is a better material for rigid pavement applications, with a percentage of compressive strength loss of 7.38% to 21.94% for OPC concrete. This current study contributes to the field of knowledge by providing a reference for future development of fly ash based geopolymer for rigid pavement applications.

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Mitigation of environmental problems using brick kiln rice husk ash in geopolymer composites for sustainable development

2021 , Shaik Numan Mahdi , Dushyanth V. Babu R , Shivakumar M , Mohd. Mustafa Al Bakri Abdullah

Brick kilns uses assorted amount of rice husk as fuel to fire the stacks of soil bricks. In India, the rice husk ash (RHA) created during the burning process of bricks has yet to be properly exploited. The main focus of this study is to enhance the structural properties of geopolymer composites using brick kiln incinerated rice husk ash waste. The Physico-chemical analysis of brick kiln rice husk ash indicates the presence of high silica (88%) content with the evidence of XRD and FTIR analysis, SEM images shows high porous structure and PSD analysis gives a bonding nature of particle size as binding ingredient. The geopolymer mixes were made manually with different percentage of RHA 0%, 10%, 20% and 30% replaced partially in Siliceous Flyash. To identify suitability of the mixture for geopolymer concrete production, properties like workability and fresh density of the mixture was investigated using manually casted cubes having a size of 100 mm and keeping for oven drying at 40° ±2 °C upto 24 h. Compressive strength as destructive structural test method was investigated at the respective duration of curing. The findings led to the conclusion that increasing the percentages of RHA in the combination improves the mixture for geopolymer concrete composites with the increase of curing time. At 10% RHA addition, the optimal compressive strength of 42.19 N/mm2 was achieved. The compressive strength of the RHA was found to decrease by 0.8% at 10% addition, which is negligible when compared to the control geopolymer mix (i.e., mix with 0% RHA), implying that the RHA from brick kilns can be employed to improve the structural qualities of geopolymer concrete composites.

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Cold-pressed fly ash geopolymers: effect of formulation on mechanical and morphological characteristics

2021 , Ong Shee-Ween , Heah Cheng Yong , Lynette Wei Ling Chan , Mohd. Mustafa Al Bakri Abdullah , Ho Li Ngee , Liew Yun Ming , Ooi Wan-En , Ng Yong-Sing , Nur Ain Jaya

This research uses low alkali activator content and cold pressing technique for fly ash-based geopolymers formation under room temperature condition. The geopolymers were prepared using four different parameters: fly ash/alkali activator ratio, sodium hydroxide concentration, sodium silicate/sodium hydroxide ratio and pressing force. The results indicated that the compressive strength (114.2 MPa) and flexural strength (29.9 MPa) of geopolymers maximised at a fly ash/alkali activator ratio of 5.5, a 14 M sodium hydroxide concentration, a sodium silicate/sodium hydroxide ratio of 1.5 and a pressing force of 5 tons (pressing stress of 100.0 MPa and 155.7 MPa for compressive and flexural samples, respectively). The degree of reaction (40.1%) enhanced the structure compactness with minimum porosity. The improved mechanical properties confirmed that a high strength pressed geopolymer could be formed at low alkali activator content without the aid of temperature.

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Contribution of interfacial bonding towards geopolymers properties in geopolymers reinforced fibers: A review

2022 , Muhd Hafizuddin Yazid , Meor Ahmad Faris bin Meor Ahmad Tajudin , Mohd. Mustafa Al Bakri Abdullah , Marcin Nabiałek , Shayfull Zamree Abd. Rahim , Mohd Arif Anuar Mohd Salleh , Marwan Kheimi , Andrei Victor Sandu , Adam Rylski , Bartłomiej Jeż

There is a burgeoning interest in the development of geopolymers as sustainable construction materials and incombustible inorganic polymers. However, geopolymers show quasi-brittle behavior. To overcome this weakness, hundreds of researchers have focused on the development, characterization, and implementation of geopolymer-reinforced fibers for a wide range of applications for light geopolymers concrete. This paper discusses the rapidly developing geopolymer-reinforced fibers, focusing on material and geometrical properties, numerical simulation, and the effect of fibers on the geopolymers. In the section on the effect of fibers on the geopolymers, a comparison between single and hybrid fibers will show the compressive strength and toughness of each type of fiber. It is proposed that interfacial bonding between matrix and fibers is important to obtain better results, and interfacial bonding between matrix and fiber depends on the type of material surface contact area, such as being hydrophobic or hydrophilic, as well as the softness or roughness of the surface.

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Effect of rubber sludge on the physical and mechanical properties of low calcium fly ash-based geopolymer

2025 , Tee Hoe Woon , Heah Cheng Yong , Ng Qi Hwa , Mohd. Mustafa Al Bakri Abdullah , Jia-Ni Lim , Ong Shee-Ween , O. Wan-En , Hang Yong-Jie

In this research, experimental work has been carried out to check the feasibility of using rubber sludge (RS) to partially replace fly ash (FA) in the production of geopolymer. RS is employed in this study as disposing of RS has led to an issue and is abundant, especially in countries producing rubber products. RS is classified as hazardous waste. Improper awareness on hazardous waste handling can spread a variety of diseases. Therefore, handling of hazardous waste is not easy as competent personnel is required during the collection, transportation, treatment and final disposal. As a result, the cost of disposing the hazardous waste are relatively high. With that, FA incorporated RS geopolymer will able to solve the landfill problems and used it as building materials will save costs, preserve natural resources, and protect the environment from waste impact and hazards. In this study, the physical and mechanical properties were investigated. It was used to replace fly ash at 5 wt.%, 10 wt.%, 15 wt.%, and 20 wt.%. Water absorption, apparent porosity, bulk density, and compressive strength were tested. The test result shows that 5 wt.% of RS incorporation to fly ash-based geopolymer is optimum as it has 1752 kg/m3 of density, 9.5% of water absorption, 19.2% of apparent porosity, and 49.9 MPa of compressive strength.

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Contribution of interfacial bonding towards geopolymers properties in geopolymers reinforced fibers: a review

2022 , Muhd Hafizuddin Yazid , Meor Ahmad Faris bin Meor Ahmad Tajudin , Mohd. Mustafa Al Bakri Abdullah , Marcin Nabiałek , Shayfull Zamree Abd. Rahim , Mohd Arif Anuar Mohd Salleh , Marwan Kheimi , Andrei Victor Sandu , Adam Rylski , Bartłomiej Jeż

There is a burgeoning interest in the development of geopolymers as sustainable construction materials and incombustible inorganic polymers. However, geopolymers show quasi-brittle behavior. To overcome this weakness, hundreds of researchers have focused on the development, characterization, and implementation of geopolymer-reinforced fibers for a wide range of applications for light geopolymers concrete. This paper discusses the rapidly developing geopolymer-reinforced fibers, focusing on material and geometrical properties, numerical simulation, and the effect of fibers on the geopolymers. In the section on the effect of fibers on the geopolymers, a comparison between single and hybrid fibers will show the compressive strength and toughness of each type of fiber. It is proposed that interfacial bonding between matrix and fibers is important to obtain better results, and interfacial bonding between matrix and fiber depends on the type of material surface contact area, such as being hydrophobic or hydrophilic, as well as the softness or roughness of the surface.

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The effect of particle size on the mechanical properties of Alkali Activated Steel Slag Mortar

2022 , Doh Shu Ing , Ho Chia Min , Xiaofeng Li , Ramadhansyah Putra Jaya , Mohd. Mustafa Al Bakri Abdullah , Siew Choo Chin , Nur Liza Rahim , Marcin Nabiałek

With the rapid development of industry, abundant industrial waste has resulted in escalating environmental issue. Steel slag is the by-product of steel-making and can be used as cementitious materials in construction. However, the low activity of steel slag limits its utilization. Much investigation has been conducted on steel slag, while only a fraction of the investigation focuses on the effect of steel slag particle size on the properties of mortar. The aim of this study is to investigate the effect of steel slag particle size as cement replacement on properties of steel slag mortar activated by sodium sulphate (Na 2 SO 4). In this study, two types of steel slag, classified as fine steel slag (FSS) with particle sizes of 0.075mm and coarse steel slag (CSS) with particle sizes of 0.150 mm, were used for making alkali activated steel slag (AASS) mortar. Flow table test, compressive strength test, flexural strength test and UPV test were carried out by designing and producing AASS mortar cubes of (50 × 50 × 50) mm at 0, 10%, 20% and 30% replacement ratio and at 0.85% addition of Na 2 SO 4. The results show that the AASS mortar with FSS possess a relatively good strength in AASS mortar. AASS mortar with FSS which is relatively finer shows a higher compressive strength than CSS up to 38.0% with replacement 52 DOH SHU ING et al. ratio from 10% to 30%. This study provided the further investigation on the combined influence of replacement ratio and particle size of SS in the properties of fresh and hardened AASS.