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  5. Infrared spectroscopy of extracted and acetylated chitin in versatile deep eutectic solvents (DES)
 
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Infrared spectroscopy of extracted and acetylated chitin in versatile deep eutectic solvents (DES)

Journal
AIP Conference Proceedings
ISSN
0094243X
Date Issued
2022-05-18
Author(s)
Suhardy Daud
Universiti Malaysia Perlis
Luqman Musa
Universiti Malaysia Perlis
Farizul Hafiz Kasim
Universiti Malaysia Perlis
Mohd Nazry Salleh
Universiti Malaysia Perlis
Nazahah Mustafa
Universiti Malaysia Perlis
Ahmad Z.
DOI
10.1063/5.0090914
Abstract
The conventional method to extract the chitin content from the crustacean shells usually uses concentrated acids and alkalis to remove impurities such as calcium carbonate and protein. However, the uses of concentrated acids and alkalis have caused many environmental issues. Deep Eutectic Solvent (DES) is one of the solvents that can be used to extract the chitin content from the crustacean shells. DES has two components namely Hydrogen Bond Donor (HBD) and Hydrogen Bond Acceptor (HBA). In this study, two types of DES have been used are betaine (HBA) - urea (HBD) and choline chloride (HBA) - urea (HBD). The results showed that DES betaine - urea and choline chloride - urea have extracted chitin content of 5.4609 % and 2.0020 % w/w respectively. The extracted chitins were analyzed using infrared spectroscopy method. The values of the degree of acetylation (DA) for the chitins were 103.1699 and 83.4821 respectively.
File(s)
Research repository notification.pdf (4.4 MB)
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