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  5. Influence of sintering temperature on density, hardness, shrinkage and microstructure of Alumina-Zirconia cutting tool
 
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Influence of sintering temperature on density, hardness, shrinkage and microstructure of Alumina-Zirconia cutting tool

Journal
International Journal of Nanoelectronics and Materials (IJNeaM)
ISSN
1985-5761
Date Issued
2021-08
Author(s)
A. A. Anis
Universiti Teknikal Malaysia Melaka
A. B. Hadzley
Universiti Teknikal Malaysia Melaka
A. A Umar
Universiti Teknikal Malaysia Melaka
T.Norfauzi
Universiti Teknikal Malaysia Melaka
M. R. Fairuz
Jabatan Keselamatan dan Kesihatan Pekerjaan Melaka
S. G. Herawan
Bina Nusantara University
K. Thongkaew
Prince of Songkla University
Handle (URI)
https://ijneam.unimap.edu.my/
https://hdl.handle.net/20.500.14170/13901
Abstract
The confederation of Alumina (Al₂O₃) and Zirconia (ZrO₂) has emerged as a promising ceramic framework for advanced machine tool applications. The mechanical properties of the Al₂O₃-ZrO2 cutting tool are critically dependent on its density, hardness, and shrinkage, which are influenced by the powder preparation and sintering processes. The effect of sintering temperature on density, hardness, shrinkage, and microstructure of Al₂O₃-ZrO₂ is investigated in this study. Al₂O₃ powders (80% wt) and ZrO₂ powders (20% wt) were combined in a ball mill machine with polyethylene glycol (PEG) added as a binder agent. The samples were compacted using the cold isostatic pressing method at 300 MPa pressure after being pressed using a hydraulic hand press machine at 10 tons pressure. The green compacts were sintered at temperatures ranging from 1500°C to 1700°C, with soaking times ranging from 4 to 6 hours. The results show that as the sintering temperature increased, the density and hardness decreased. When the sintering temperature was set to 1500°C and the soaking time was 6 hours, the maximum hardness and density were recorded at 1321.23HV. Whereas, lowest hardness was recorded at 688.4HV when the sintering temperature was set to 1700°C and the soaking time was 6 hours. The shrinkage increased significantly as the sintering temperature increased, reaching a maximum of 9.95 percent at 1700°C after 4 hours of soaking. Microstructure analysis reveals that grain size increased as sintering temperature increased, with the smallest grain size presented 2 μm at 1500°C and 6 hours of soaking time.
Subjects
  • Alumina

  • Zirconia

  • Density

  • Hardness

  • Shrinkage

  • Microstructure

File(s)
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Acquisition Date
Mar 5, 2026
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Mar 5, 2026
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