Zunaida Zakaria
Thumbnail Image
Preferred name
Zunaida Zakaria
Official Name
Zunaida, Zakaria
Alternative Name
Zakaria, Zunaida
Zunaida, Z.
Zakaria, Z.
Main Affiliation
Scopus Author ID
57217205824
Researcher ID
M-6958-2019

Research Output

Filters

1
1
1
1
Reset filters

Settings
Now showing 1 - 1 of 1
  • Publication
    Development of porous epoxy micro-beads using ammonium bicarbonate through a single epoxy droplet in corn oil
    ( 2021-01-01)
    Leemsuthep A.
    ;
    Zunaida Zakaria
    ;
    Tanrattanakul V.
    ;
    Ramarad S.
    ;
    Muniyadi M.
    ;
    Jaruga T.
    ;
    Munusamy Y.
    ;
    Wnuk I.
    ;
    Pietrusiewicz P.
    This paper explored the effects of ammonium bicarbonate and different ratios of epoxy to polyamide on the formation of porous epoxy micro-beads through a single epoxy droplet. A single drop of a mixture, consisting of epoxy, polyamide, and ammonium bicarbonate, was dropped into heated corn oil at a temperature of 100 °C. An epoxy droplet was formed due to the immiscibility of the epoxy mixture and corn oil. The ammonium bicarbonate within this droplet underwent a decomposition reaction, while the epoxy and polyamide underwent a curing reaction, to form porous epoxy micro-beads. The result showed that the higher ammonium bicarbonate content in the porous, epoxy micro-beads increased the decomposition rate up to 11.52 × 10−3 cm3/s. In addition, a higher total volume of gas was generated when a higher ammonium bicarbonate content was de-composed. This led to the formation of porous epoxy micro-beads with a smaller particle size, lower specific gravity, and better thermal stability. At an epoxy to polyamide ratio of 10:6, many smaller micro-beads, with particle sizes ranging from 201 to 400 μm, were obtained at an ammonium bicar-bonate content of 10 phr. Moreover, the porous epoxy micro-beads with open pores were shown to have a low specific gravity of about 0.93 and high thermal stability at a high ammonium bicarbonate content. Based on the findings, it was concluded that porous epoxy micro-beads were successfully produced using a single epoxy droplet in heated corn oil, where their shape and particle size de-pended on the content of ammonium bicarbonate and the ratio of epoxy to polyamide used.
      1  27