Siti Khalijah Mahmad Rozi
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Siti Khalijah Mahmad Rozi
Official Name
Siti Khalijah, Mahmad Rozi
Alternative Name
Rozi, Siti Khalijah Mahmad
Rozi, S.K.M
Mahmad Rozi, S.K
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Scopus Author ID
57190815094

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Asam gelugur-based carbon aerogels for highly recyclable oils adsorption

2023-07 , Cheong Yi Xin , Siti Khalijah Mahmad Rozi , Monisha Devi Elan Solan , Syazwani Mahmad Puzi

Rapid development of the oil industries and improper oil management caused a huge amount of oil pollutant released into the water environment. Oil pollutant is toxic and may harm aquatic biodiversity. The present work highlights the facile preparation of carbon aerogels based from Asam Gelugur (CA@Ga) for oil remediation from aqueous. Analysis on the structure of CA@Ga using Fourier Transform Infrared Spectroscopy (FTIR), Energy Dispersive X-ray (EDX) and Scanning Electron Microscopy (SEM), confirmed the successful preparation of CA@Ga through hydrothermal carbonization. The main parameters affecting the adsorption of oil such as the sorption time, pH and mass of sorbent were screened and oil adsorption studies revealed that the optimum conditions were at contact time of 3 minutes, pH of solution at 7 and the adsorbent mass of 2 g with the highest adsorption capacity of 0.82 + 0.01 g/g. CA@Ga displayed a good stability towards thermal treatment and exhibited good adsorption ability towards several types of oil. Recyclability study depicts that CA@Ga could be regenerated by simple physical treatments and retained a high sorption after 10 cycles with adsorption capacity of 0.80 + 0.01 g/g. Therefore, the prepared CA@Ga has potential in application of oil recovery and environmental protection.

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Activated carbon derived from Jackfruit seeds for oil adsorption

2024-07 , Zi Ching Chan , Hairul Nazirah Abdul Halim , Siti Khalijah Mahmad Rozi

Activated carbons (AC) are widely used as adsorbents for treating oily wastewater. An effective, cheap and environmental-friendly method for oil adsorption by using AC derived from jackfruit seeds (JS) was developed in this study. The JS were chemically activated with different concentrations (10 wt.% and 15 wt.%) of chemical activating agents (H3PO4 and ZnCl2) to produce activated carbon. The optimum conditions for developing AC from JS with the highest oil adsorption capacity was found using 15 wt.% ZnCl2, and carbonised at 500°C resulting in maximum adsorption capacity of 0.8621 g/g. Raw JS and jackfruit seed-derived activated carbon (JSAC) were characterized by Fourier Transform Infrared Spectroscopy and Scanning Electron Microscopy analysis. The influence of process parameters such as contact times (0 – 240 minutes), adsorbent dosages (0.5 – 2.5 g) and adsorption temperatures (25 – 65 °C) for oil adsorption were investigated. The results showed that the optimum parameters for maximum adsorption capacity were as follows; 120 minutes of contact time, adsorbent dosage of 1.5 g and at 35 °C. At this condition, the highest oil adsorption capacity was achieved at 1.5674 g/g. The adsorption kinetic studies depicted that the oil adsorption mechanism was represented by pseudo-second-order kinetic model which implies that the adsorption is a chemisorption process. Jackfruit seeds had been proven to have the capability as an effective adsorbent for oil adsorption.

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Publication

Asam Gelugur-based carbon aerogels for highly recyclable oils adsorption

2023-07 , Cheong Yi Xin , Siti Khalijah Mahmad Rozi , Monisha Devi Elan Solan , Syazwani Mahmad Puzi

Rapid development of the oil industries and improper oil management causeda huge amount of oil pollutant released into the water environment. Oil pollutant is toxic and may harm aquatic biodiversity. The present work highlights the facile preparation of carbon aerogels basedfromAsam Gelugur (CA@Ga) for oil remediation from aqueous. Analysis on the structure of CA@Gausing Fourier Transform Infrared Spectroscopy (FTIR), Energy Dispersive X-ray (EDX) and Scanning Electron Microscopy (SEM), confirmed the successful preparation of CA@Ga through hydrothermal carbonization. The main parameters affecting the adsorption of oil such as the sorption time, pH and mass of sorbent were screened and oil adsorption studies revealed that the optimum conditions were at contact time of 3 minutes, pH of solution at 7 and the adsorbent mass of 2 g with the highest adsorption capacity of 0.82 +0.01 g/g.CA@Ga displayed a good stability towards thermal treatment and exhibited good adsorption ability towards several types of oil. Recyclability study depicts that CA@Ga could be regenerated by simple physical treatments and retaineda high sorption after 10 cycles with adsorption capacity of 0.80 +0.01 g/g. Therefore, the prepared CA@Ga has potential in application of oil recovery and environmental protection.

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Publication

Asam Gelugur-based carbon aerogels for highly recyclable oil adsorption

2023-07 , Cheong Yi Xin , Siti Khalijah Mahmad Rozi , Monisha Devi Elan Solan , Syazwani Mahmad Puzi

Rapid development of the oil industries and improper oil management causeda huge amount of oil pollutant released into the water environment. Oil pollutant is toxic and may harm aquatic biodiversity. The present work highlights the facile preparation of carbon aerogels basedfromAsam Gelugur (CA@Ga) for oil remediation from aqueous. Analysis on the structure of CA@Gausing Fourier Transform Infrared Spectroscopy (FTIR), Energy Dispersive X-ray (EDX) and Scanning Electron Microscopy (SEM), confirmed the successful preparation of CA@Ga through hydrothermal carbonization. The main parameters affecting the adsorption of oil such as the sorption time, pH and mass of sorbent were screened and oil adsorption studies revealed that the optimum conditions were at contact time of 3 minutes, pH of solution at 7 and the adsorbent mass of 2 g with the highest adsorption capacity of 0.82 +0.01 g/g.CA@Ga displayed a good stability towards thermal treatment and exhibited good adsorption ability towards several types of oil. Recyclability study depicts that CA@Ga could be regenerated by simple physical treatments and retaineda high sorption after 10 cycles with adsorption capacity of 0.80 +0.01 g/g. Therefore, the prepared CA@Ga has potential in application of oil recovery and environmental protection

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