Now showing 1 - 8 of 8
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Production and characterization of graphene from carbonaceous rice straw by cost-effect extraction

2021-05-01 , Muhammad Nur Aiman Uda , Subash Chandra Bose Gopinath , Uda Hashim , Halim N.H. , Nor Azizah Parmin , Muhammad Nur Afnan Uda , Anbu P.

This paper describes the synthesis of graphene-based activated carbon from carbonaceous rice straw fly ash in an electrical furnace and the subsequent potassium hydroxide extraction. The produced graphene has a proper morphological structure; flakes and a rough surface can be observed. The average size of the graphene was defined as up to 2000 nm and clarification was provided by high-resolution microscopes (FESEM and FETEM). Crystallinity was confirmed by surface area electron diffraction. The chemical bonding from the graphene was clearly observed, with –C=C– and O–H stretching at peaks of 1644 cm−1 and 3435 cm−1, respectively. Impurities in the graphene were found using X-ray photoelectron spectroscopy and energy dispersive X-ray spectroscopy. The measured size, according to zeta-potential analysis, was 8722.2 ± 25 nm, and the average polydispersity index was 0.576. The stability of the mass reduction was analyzed by a thermogravimetric at 100 Â°C, with a final reduction of ~ 11%.

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Home automation system for security and temperature control using microcontroller based with smartphone applications

2021-05-03 , Muhammad Aizat Abu Bakar , Fazreen Mohd Yusoff , Aminudin Anuar , Muhammad Nur Aiman Uda , Asyraf Hakimi Abu Bakar , Muhammad Nur Afnan Uda , Mohamed K. Sulaiman

In Malaysia, the El-Nino phenomenon happen in 2016 was caused the used of home appliances increasing including air-conditioner, fan and air cooler which are used frequently compared to other appliances. This report presents prototype development System for Security and Temperature Control using Microcontroller Based with Smartphone Application. The system has beneficial to reduce human labour besides energy saving and designed for special purposes which can easily maintain the temperature in sorrounding home. The system used several sensors for input parts including LM35 for temperature sensor and Passive Infra-Red (PIR) sensor for motion detector. For security system, the Radio-frequency Identification (RFID) has been used as security input user identification. A microcontroller arduino uno type is used as the system brain in the process part. In outputs part, servo motor has been used as door application while Light-Emitting Diode (LED) and buzzer as indicators when RFID is in use. A smartphone application is implemented in the system which allows the user to control a device remotely including home appliances through Bluetooth module. All data will display in Liquid Crystal Display (LCD) as user reference.

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Silica and graphene mediate arsenic detection in mature rice grain by a newly patterned current–volt aptasensor

2021-12-01 , Muhammad Nur Aiman Uda , Subash Chandra Bose Gopinath , Uda Hashim , Halim N.H. , Nor Azizah Parmin , Muhammad Nur Afnan Uda , Anbu P. , Tijjani Adam

Arsenic is a major global threat to the ecosystem. Here we describe a highly accurate sensing platform using silica nanoparticles/graphene at the surface of aluminum interdigitated electrodes (Al IDE), able to detect trace amounts of arsenic(III) in rice grain samples. The morphology and electrical properties of fabricated Al IDEs were characterized and standardized using AFM, and SEM with EDX analyses. Micrometer scale Al IDEs were fabricated with silicon, aluminum, and oxygen as primary elements. Validation of the bare Al IDE with electrolyte fouling was performed at different pH levels. The sensing surface was stable with no electrolyte fouling at pH 7. Each chemical modification step was monitored with current–volt measurement. The surface chemical bonds were characterized by fourier transform infrared spectroscopy (FTIR) and revealed different peaks when interacting with arsenic (1600–1000 cm−1). Both silica nanoparticles and graphene presented a sensitive limit of detection as measured by slope calibration curves at 0.0000001 pg/ml, respectively. Further, linear regression was established using ΔI (A) = 3.86 E−09 log (Arsenic concentration) [g/ml] + 8.67 E−08 [A] for silica nanoparticles, whereas for graphene Y = 3.73 E−09 (Arsenic concentration) [g/ml] + 8.52 E−08 on the linear range of 0.0000001 pg/ml to 0.01 pg/ml. The R2 for silica (0.96) and that of graphene (0.94) was close to the maximum (1). Modification with silica nanoparticles was highly stable. The potential use of silica nanoparticles in the detection of arsenic in rice grain extract can be attributed to their size and stability.

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Novelty Studies on Amorphous Silica Nanoparticle Production from Rice Straw Ash

2020-07-09 , Muhammad Nur Aiman Uda , Subash Chandra Bose Gopinath , Uda Hashim , Muhammad Nur Afnan Uda , Nor Azizah Parmin , Halim N.H. , Anbu P.

Turning waste product into the valuable resources is the best alternative way to overcome the waste management issue. Generally, rice is grown and planted twice a year where a lot of rice by-products have been produced after harvesting the matured paddy. Rice straw is one of turning waste products into the valuable resources and to manage the environmental issues. Generally, rice is grown and planted twice a year where a lot of rice by-products are produced. Rices straw is one of the rice by-products, generated roughly 0.7-1.4 kg per kilograms of harvested milled rice. With the nanotechnological approach, silica particles at nano-size can be produced using the incinerated rice straw. In addition to that, this research will report the synthesis, characterization and adsorption analysis towards the heavy metal removal.

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Arthropods-mediated Green Synthesis of Zinc Oxide Nanoparticles using Cellar Spider Extract: A Biocompatible Remediation for Environmental Approach

2024-06-12 , Muzamir Isa , Muhammad Nur Aiman Uda , Irfan M.A.R. , Uda Hashim , Subash Chandra Bose Gopinath , Hafiza Shukor , Afnan Uda M.N. , Huzaifah M.R.M. , Ali M.M. , Ibrahim N.H. , Makhtar M.M.Z. , Ng Q.H. , Mohd Khairul Rabani Hashim , Zainal Abidin Arsat , Nor Azizah Parmin , Liyana Ahmad Sofri , Ruslan M.A.M. , Tijjani Adam

This study presents an eco-friendly approach to synthesizing zinc oxide nanoparticles (ZnO NPs) using extracts from cellar spiders, addressing environmental and health concerns associated with conventional methods. The spider extract efficiently reduced zinc acetate dihydrate, and the synthesized ZnO NPs underwent comprehensive quantitative characterization, including size, shape, morphology, surface chemistry, thermal stability, and optical properties using Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), zeta potential measurements, thermogravimetric analysis (TGA), and UV-vis spectroscopy. The nanoparticles exhibited intended characteristics, and their adsorption capability for methylene blue (MB) was quantitatively assessed using the Freundlich isotherm model and pseudo-second-order kinetic model, providing numerical insights into MB removal efficiency. The study demonstrates the potential of these green-synthesized ZnO NPs for applications in environmental remediation, wastewater treatment, and antibacterial therapies, contributing to both sustainable nanomaterial development and quantitative understanding of their functional properties.

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Analysis on Silica and Graphene Nanomaterials Obtained From Rice Straw for Antimicrobial Potential

2024-06-12 , Muhammad Nur Aiman Uda , A Jalil N.H. , Muhammad Firdaus Abdul Muttalib , Fadhilnor Abdullah , Uda Hashim , Subash Chandra Bose Gopinath , Afnan Uda M.N. , Shahidah Arina Shamsuddin , Norizah Abd Karim , Ahmad Radi Wan Yaakub , Ibrahim N.H. , Tijjani Adam , Nor Azizah Parmin , Baharum N.A.

This study focuses on the encapsulation of silica and graphene nanoparticles and their potential applications. The encapsulation enhances the properties and effectiveness of these nanoparticles, with silica providing stability and graphene contributing to high surface area and electrical conductivity. Characterization of silica-graphene nanoparticles was conducted using various techniques including High Power Microscope (HPM), Scanning Electron Microscope (SEM), Energy-dispersive X-ray spectroscopy (EDS), and 3D Nano Profiler. The antimicrobial activity of silica, graphene, and silica-graphene nanoparticles was evaluated using a disc diffusion assay against E. coli and B. subtilis at varying concentrations. Results showed significant antimicrobial activity, with the inhibition zone being directly proportional to the concentration. Silica-graphene nanoparticles demonstrated higher efficacy against E. coli compared to B. subtilis, attributed to differences in cell wall structure. Statistical analysis using ANOVA confirmed significant differences in antimicrobial activity among the tested components.

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Synthesis of Zinc Oxide Nanoparticles via Cellar Spider Extract for Enhanced Functional Properties in Antimicrobial Activities

2024-06-12 , Jasni Mohamed Ismail , Muhammad Nur Aiman Uda , Irfan Abd Rahim , Mohd Khairul Rabani Hashim , Zainal Abidin Arsat , Uda Hashim , Hafiza Shukor , Afnan Uda M.N. , Ibrahim N.H. , Shahidah Arina Shamsuddin , Nor Azizah Parmin , Muzamir Isa , Zain M.Z.M. , Ilyas R.A. , Tijjani Adam

This study explores the green synthesis of zinc oxide nanoparticles (ZnO NPs) using cellar spider extracts as a sustainable alternative to traditional methods involving hazardous chemicals and radiation. The spider extracts effectively reduced zinc acetate dihydrate, yielding white precipitates indicative of ZnO NPs. Characterization through SEM revealed diverse morphologies, including spherical, rod-like, hexagonal, and uneven particles forming platelet-like aggregates. Further analyses, such as HPM, 3D nanoprofiler, and EDS, provided insights into size, shape, morphology, surface chemistry, thermal stability, and optical characteristics, quantifying the intended properties of the synthesized ZnO NPs. Antibacterial assays against E. coli and B. subtilis demonstrated significant antibacterial activity, affirming the nanoparticles' potential for antimicrobial applications. This green synthesis approach, validated through comprehensive characterization and quantitative measurements, offers a promising and environmentally friendly route for producing functional ZnO NPs.

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Mycorrhiza: a natural resource assists plant growth under varied soil conditions

2020-05-01 , Huey C.J. , Subash Chandra Bose Gopinath , Muhammad Nur Aiman Uda , Zulhaimi H.I. , Jaafar M.N. , Kasim F.H. , Yaakub A.R.W.

In this overview, the authors have discussed the potential advantages of the association between mycorrhizae and plants, their mutual accelerated growth under favorable conditions and their role in nutrient supply. In addition, methods for isolating mycorrhizae are described and spore morphologies and their adaptation to various conditions are outlined. Further, the significant participation of controlled greenhouses and other supported physiological environments in propagating mycorrhizae is detailed. The reviewed information supports the lack of host- and niche-specificity by arbuscular mycorrhizae, indicating that these fungi are suitable for use in a wide range of ecological conditions and with propagules for direct reintroduction. Regarding their prospective uses, the extensive growth of endomycorrhizal fungi suggests it is suited for poor-quality and low-fertility soils.